 
data_sl97 
 
_audit_creation_method            SHELXL-97 
_chemical_name_systematic 
; 
 ? 
; 
_chemical_name_common             ? 
_chemical_melting_point           ? 
_chemical_formula_moiety          ? 
_chemical_formula_sum 
 'O17 Rb14 Si10' 
_chemical_formula_weight          1749.48 
 
loop_ 
 _atom_type_symbol 
 _atom_type_description 
 _atom_type_scat_dispersion_real 
 _atom_type_scat_dispersion_imag 
 _atom_type_scat_source 
 'Rb'  'Rb'  -0.9393   0.0000 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'Si'  'Si'   0.0817   0.0000 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'O'  'O'   0.0106   0.0000 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 
_symmetry_cell_setting            ? 
_symmetry_space_group_name_H-M    ? 
 
loop_ 
 _symmetry_equiv_pos_as_xyz 
 'x, y, z' 
 '-x, y+1/2, -z+1/2' 
 '-x, -y, -z' 
 'x, -y-1/2, z-1/2' 
 
_cell_length_a                    14.633(9) 
_cell_length_b                    7.936(4) 
_cell_length_c                    32.884(16) 
_cell_angle_alpha                 90.00 
_cell_angle_beta                  103.50(2) 
_cell_angle_gamma                 90.00 
_cell_volume                      3713(3) 
_cell_formula_units_Z             4 
_cell_measurement_temperature     293(2) 
_cell_measurement_reflns_used     ? 
_cell_measurement_theta_min       ? 
_cell_measurement_theta_max       ? 
 
_exptl_crystal_description        ? 
_exptl_crystal_colour             ? 
_exptl_crystal_size_max           ? 
_exptl_crystal_size_mid           ? 
_exptl_crystal_size_min           ? 
_exptl_crystal_density_meas       ? 
_exptl_crystal_density_diffrn     3.129 
_exptl_crystal_density_method     'not measured' 
_exptl_crystal_F_000              3176 
_exptl_absorpt_coefficient_mu     18.642 
_exptl_absorpt_correction_type    ? 
_exptl_absorpt_correction_T_min   ? 
_exptl_absorpt_correction_T_max   ? 
_exptl_absorpt_process_details    ? 
 
_exptl_special_details 
; 
 ? 
; 
 
_diffrn_ambient_temperature       293(2) 
_diffrn_radiation_wavelength      0.71073 
_diffrn_radiation_type            MoK\a 
_diffrn_radiation_source          'fine-focus sealed tube' 
_diffrn_radiation_monochromator   graphite 
_diffrn_measurement_device_type   ? 
_diffrn_measurement_method        ? 
_diffrn_detector_area_resol_mean  ? 
_diffrn_standards_number          ? 
_diffrn_standards_interval_count  ? 
_diffrn_standards_interval_time   ? 
_diffrn_standards_decay_%         ? 
_diffrn_reflns_number             10536 
_diffrn_reflns_av_R_equivalents   0.1053 
_diffrn_reflns_av_sigmaI/netI     0.3732 
_diffrn_reflns_limit_h_min        -19 
_diffrn_reflns_limit_h_max        10 
_diffrn_reflns_limit_k_min        -10 
_diffrn_reflns_limit_k_max        10 
_diffrn_reflns_limit_l_min        -39 
_diffrn_reflns_limit_l_max        35 
_diffrn_reflns_theta_min          1.27 
_diffrn_reflns_theta_max          28.22 
_reflns_number_total              7773 
_reflns_number_gt                 2208 
_reflns_threshold_expression      >2sigma(I) 
 
_computing_data_collection        ? 
_computing_cell_refinement        ? 
_computing_data_reduction         ? 
_computing_structure_solution     'SHELXS-97 (Sheldrick, 1990)' 
_computing_structure_refinement   'SHELXL-97 (Sheldrick, 1997)' 
_computing_molecular_graphics     ? 
_computing_publication_material   ? 
 
_refine_special_details 
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
; 
 
_refine_ls_structure_factor_coef  Fsqd  
_refine_ls_matrix_type            full 
_refine_ls_weighting_scheme       calc  
_refine_ls_weighting_details 
 'calc w=1/[σ²(Fo²)+(0.0753P)²+0.0000P] where P=(Fo²+2Fc²)/3' 
_atom_sites_solution_primary      direct 
_atom_sites_solution_secondary    difmap 
_atom_sites_solution_hydrogens    geom 
_refine_ls_hydrogen_treatment     mixed 
_refine_ls_extinction_method      SHELXL 
_refine_ls_extinction_coef        0.00153(9) 
_refine_ls_extinction_expression 
 'Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^' 
_refine_ls_number_reflns          7773 
_refine_ls_number_parameters      371 
_refine_ls_number_restraints      0 
_refine_ls_R_factor_all           0.2195 
_refine_ls_R_factor_gt            0.0767 
_refine_ls_wR_factor_ref          0.2089 
_refine_ls_wR_factor_gt           0.1718 
_refine_ls_goodness_of_fit_ref    0.707 
_refine_ls_restrained_S_all       0.707 
_refine_ls_shift/su_max           0.000 
_refine_ls_shift/su_mean          0.000 
 
loop_ 
 _atom_site_label 
 _atom_site_type_symbol 
 _atom_site_fract_x 
 _atom_site_fract_y 
 _atom_site_fract_z 
 _atom_site_U_iso_or_equiv 
 _atom_site_adp_type 
 _atom_site_occupancy 
 _atom_site_symmetry_multiplicity 
 _atom_site_calc_flag 
 _atom_site_refinement_flags 
 _atom_site_disorder_assembly 
 _atom_site_disorder_group 
Rb1 Rb 0.05292(16) 0.4889(3) 0.25811(8) 0.0311(6) Uani 1 1 d . . . 
Rb2 Rb 0.05802(18) 0.0097(3) 0.06645(8) 0.0390(7) Uani 1 1 d . . . 
Rb3 Rb 0.06111(17) 0.1381(3) 0.36069(8) 0.0322(7) Uani 1 1 d . . . 
Rb4 Rb 0.15885(18) 0.4843(3) 0.10812(9) 0.0385(7) Uani 1 1 d . . . 
Rb5 Rb 0.20380(16) 0.5526(3) 0.38434(8) 0.0296(6) Uani 1 1 d . . . 
Rb6 Rb 0.28936(16) 0.6364(3) 0.21521(8) 0.0272(6) Uani 1 1 d . . . 
Rb7 Rb 0.30671(17) 0.5305(3) 0.62867(8) 0.0346(7) Uani 1 1 d . . . 
Rb8 Rb 0.33724(17) 0.0543(3) 0.39016(8) 0.0348(7) Uani 1 1 d . . . 
Rb9 Rb 0.4065(2) 0.6299(3) 0.03305(9) 0.0450(8) Uani 1 1 d . . . 
Rb10 Rb 0.43563(17) 0.4009(3) 0.14465(8) 0.0315(7) Uani 1 1 d . . . 
Rb11 Rb 0.44628(16) 0.0529(3) 0.24248(8) 0.0297(6) Uani 1 1 d . . . 
Rb12 Rb 0.51553(18) 0.0430(3) 0.06609(8) 0.0348(7) Uani 1 1 d . . . 
Rb13 Rb 0.79135(16) 0.4022(3) 0.21231(8) 0.0284(6) Uani 1 1 d . . . 
Rb14 Rb 0.8846(3) 0.3674(4) 0.02786(10) 0.0704(12) Uani 1 1 d . . . 
Si1 Si 0.0087(5) 0.2381(8) 0.1540(2) 0.0244(17) Uani 1 1 d . . . 
Si2 Si 0.1124(5) 0.6042(8) 0.6760(2) 0.0260(16) Uani 1 1 d . . . 
Si3 Si 0.2159(5) 0.2280(8) 0.2018(2) 0.0245(17) Uani 1 1 d . . . 
Si4 Si 0.2753(4) 0.3155(8) 0.3006(2) 0.0211(16) Uani 1 1 d . . . 
Si5 Si 0.4863(5) 0.2932(8) 0.3403(2) 0.0225(17) Uani 1 1 d . . . 
Si6 Si 0.6124(5) 0.1403(8) 0.1733(2) 0.0202(16) Uani 1 1 d . . . 
Si11 Si 0.1575(7) 0.2891(12) 0.4770(3) 0.073(3) Uani 1 1 d . . . 
Si12 Si 0.2592(7) 0.5114(9) 0.5072(3) 0.058(3) Uani 1 1 d . . . 
Si13 Si 0.2693(6) 0.2550(9) 0.0418(2) 0.042(2) Uani 1 1 d . . . 
Si14 Si 0.3260(8) 0.2723(13) 0.4803(3) 0.070(3) Uani 1 1 d . . . 
O10 O 0.0094(11) 0.7915(19) 0.3942(6) 0.036(5) Uani 1 1 d . . . 
O11 O 0.0692(12) 0.796(2) 0.3219(6) 0.049(6) Uani 1 1 d . . . 
O12 O 0.0238(10) 0.0277(18) 0.1576(5) 0.029(4) Uani 1 1 d . . . 
O13 O 0.1125(10) 0.3105(16) 0.1798(5) 0.022(4) Uani 1 1 d . . . 
O20 O 0.0860(11) 0.778(2) 0.2103(5) 0.042(5) Uani 1 1 d . . . 
O21 O 0.1381(11) 0.8009(19) 0.1369(5) 0.032(4) Uani 1 1 d . . . 
O23 O 0.2028(10) 0.0222(18) 0.1989(5) 0.032(4) Uani 1 1 d . . . 
O30 O 0.3009(13) 0.289(2) 0.1832(7) 0.058(6) Uani 1 1 d . . . 
O34 O 0.2340(11) 0.281(2) 0.2531(6) 0.044(5) Uani 1 1 d . . . 
O40 O 0.2076(11) 0.2555(19) 0.3281(5) 0.036(5) Uani 1 1 d . . . 
O45 O 0.3778(10) 0.2275(18) 0.3141(5) 0.027(4) Uani 1 1 d . . . 
O46 O 0.2928(10) 0.5213(19) 0.3051(4) 0.026(4) Uani 1 1 d . . . 
O50 O 0.5078(11) 0.2281(19) 0.3873(5) 0.029(4) Uani 1 1 d . . . 
O51 O 0.5612(9) 0.2347(18) 0.3162(5) 0.023(4) Uani 1 1 d . . . 
O56 O 0.5247(10) 0.0077(18) 0.1601(4) 0.026(4) Uani 1 1 d . . . 
O60 O 0.5971(12) 0.258(2) 0.2086(5) 0.039(5) Uani 1 1 d . . . 
O61 O 0.6319(11) 0.2242(18) 0.1335(5) 0.030(4) Uani 1 1 d . . . 
 
 
_geom_special_details 
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
; 
 
loop_ 
 _geom_bond_atom_site_label_1 
 _geom_bond_atom_site_label_2 
 _geom_bond_distance 
 _geom_bond_site_symmetry_2 
 _geom_bond_publ_flag 
Rb1 O20 2.885(17) . ? 
Rb1 O20 2.999(19) 2_545 ? 
Rb1 O34 3.158(17) . ? 
Rb1 O11 3.188(18) . ? 
Rb1 O11 3.20(2) 2_545 ? 
Rb1 O13 3.233(16) . ? 
Rb1 O12 3.238(16) 2 ? 
Rb1 O40 3.379(16) . ? 
Rb1 O46 3.499(14) . ? 
Rb1 Si4 3.508(7) . ? 
Rb1 Si2 3.679(8) 3_566 ? 
Rb1 Si1 3.781(8) 2 ? 
Rb2 O21 2.867(17) 1_545 ? 
Rb2 O10 2.871(17) 2_545 ? 
Rb2 O12 3.157(16) . ? 
Rb2 Si11 3.599(10) 2_545 ? 
Rb2 Si1 3.615(8) . ? 
Rb2 Si2 3.618(8) 4_565 ? 
Rb2 Rb7 3.749(4) 4_565 ? 
Rb2 Rb14 3.821(4) 1_455 ? 
Rb2 Si12 3.894(11) 4_565 ? 
Rb2 Si13 3.895(9) . ? 
Rb2 Si11 3.915(12) 4_565 ? 
Rb2 Rb4 4.159(4) . ? 
Rb3 O40 2.773(17) . ? 
Rb3 O20 2.995(16) 2_545 ? 
Rb3 O11 3.013(17) 1_545 ? 
Rb3 O10 3.121(17) 1_545 ? 
Rb3 O21 3.207(15) 2_545 ? 
Rb3 Si2 3.264(7) 3_566 ? 
Rb3 O12 3.334(15) 2 ? 
Rb3 Si1 3.335(7) 2_545 ? 
Rb3 Rb4 3.800(4) 2_545 ? 
Rb3 Rb5 3.876(4) . ? 
Rb3 Si11 3.940(11) . ? 
Rb3 Rb8 3.985(4) . ? 
Rb4 O21 2.727(15) . ? 
Rb4 O10 2.884(15) 2_545 ? 
Rb4 O13 2.943(16) . ? 
Rb4 O30 3.23(2) . ? 
Rb4 Si13 3.510(9) . ? 
Rb4 Si1 3.531(8) . ? 
Rb4 Si3 3.623(8) . ? 
Rb4 Rb6 3.790(4) . ? 
Rb4 Rb3 3.800(4) 2 ? 
Rb4 Rb10 4.002(4) . ? 
Rb4 Si2 4.101(8) 4_575 ? 
Rb5 O61 2.939(16) 2_655 ? 
Rb5 O40 3.006(16) . ? 
Rb5 O11 3.153(19) . ? 
Rb5 O46 3.182(15) . ? 
Rb5 O12 3.300(15) 2 ? 
Rb5 Si1 3.405(7) 2 ? 
Rb5 O10 3.496(15) . ? 
Rb5 Si4 3.682(8) . ? 
Rb5 Si6 3.701(8) 2_655 ? 
Rb5 Si11 3.882(11) . ? 
Rb5 Si14 3.933(10) . ? 
Rb6 O51 2.741(14) 2_655 ? 
Rb6 O60 2.832(16) 2_655 ? 
Rb6 O30 2.97(2) . ? 
Rb6 O46 3.085(15) . ? 
Rb6 O20 3.150(18) . ? 
Rb6 O21 3.251(16) . ? 
Rb6 O34 3.261(18) . ? 
Rb6 O23 3.309(15) 1_565 ? 
Rb6 Si2 3.324(7) 4_575 ? 
Rb6 Si3 3.411(7) . ? 
Rb6 Rb13 3.583(4) 2_655 ? 
Rb6 Si6 3.611(7) 2_655 ? 
Rb7 O21 2.874(15) 4_576 ? 
Rb7 O51 2.977(15) 3_666 ? 
Rb7 O23 3.076(17) 4_566 ? 
Rb7 O30 3.11(2) 4_566 ? 
Rb7 O56 3.130(14) 4_566 ? 
Rb7 Si5 3.275(7) 3_666 ? 
Rb7 O50 3.461(17) 3_666 ? 
Rb7 Si13 3.586(8) 4_566 ? 
Rb7 Si2 3.594(8) . ? 
Rb7 Si3 3.640(8) 4_566 ? 
Rb7 Rb2 3.749(4) 4_566 ? 
Rb7 Rb11 3.879(4) 4_566 ? 
Rb8 O61 2.800(15) 2_645 ? 
Rb8 O50 2.872(16) . ? 
Rb8 O40 2.917(16) . ? 
Rb8 O45 3.031(16) . ? 
Rb8 Si14 3.469(10) . ? 
Rb8 Si4 3.542(7) . ? 
Rb8 Si5 3.565(8) . ? 
Rb8 Rb13 3.660(4) 2_645 ? 
Rb8 Rb10 3.952(4) 2_645 ? 
Rb8 Rb9 4.047(4) 2_645 ? 
Rb8 Si6 4.052(7) 2_645 ? 
Rb9 O50 2.738(15) 2_655 ? 
Rb9 Si12 3.552(9) 4_575 ? 
Rb9 Si13 3.638(8) . ? 
Rb9 Si14 3.692(10) 4_565 ? 
Rb9 Rb12 3.697(4) 1_565 ? 
Rb9 Rb10 4.028(4) . ? 
Rb9 Rb8 4.047(4) 2_655 ? 
Rb9 Rb14 4.263(5) 3_665 ? 
Rb9 Rb9 4.387(6) 3_665 ? 
Rb9 Rb12 4.517(4) 3_665 ? 
Rb9 Rb7 4.629(4) 4_575 ? 
Rb9 Rb8 4.798(4) 4_565 ? 
Rb10 O30 2.730(17) . ? 
Rb10 O51 2.941(15) 2_655 ? 
Rb10 O50 2.990(15) 2_655 ? 
Rb10 O60 2.996(15) . ? 
Rb10 Si6 3.274(7) . ? 
Rb10 O61 3.292(16) . ? 
Rb10 Si5 3.313(7) 2_655 ? 
Rb10 O56 3.374(14) . ? 
Rb10 Si13 3.854(8) . ? 
Rb10 Rb7 3.884(4) 4_565 ? 
Rb10 Rb11 3.902(4) 2_655 ? 
Rb10 Rb8 3.952(4) 2_655 ? 
Rb11 O51 2.980(15) . ? 
Rb11 O60 2.993(17) 2_645 ? 
Rb11 O45 3.095(16) . ? 
Rb11 O30 3.145(19) . ? 
Rb11 O60 3.147(19) . ? 
Rb11 O51 3.164(15) 2_645 ? 
Rb11 O56 3.201(15) . ? 
Rb11 O23 3.524(15) . ? 
Rb11 Si3 3.603(7) . ? 
Rb11 Si5 3.668(7) . ? 
Rb11 Si5 3.727(8) 2_645 ? 
Rb11 Si6 3.760(8) . ? 
Rb12 O61 2.850(15) . ? 
Rb12 O50 2.992(15) 2_645 ? 
Rb12 O56 3.074(15) . ? 
Rb12 Si6 3.565(7) . ? 
Rb12 Si5 3.666(7) 2_645 ? 
Rb12 Rb9 3.697(4) 1_545 ? 
Rb12 Si14 3.738(11) 2_645 ? 
Rb12 Si14 3.761(11) 4_565 ? 
Rb12 Si12 3.823(10) 4_565 ? 
Rb12 Si13 3.887(9) . ? 
Rb12 Rb5 4.050(4) 2_645 ? 
Rb12 Rb7 4.104(4) 4_565 ? 
Rb13 O11 2.686(16) 2_645 ? 
Rb13 O20 2.922(17) 2_645 ? 
Rb13 O60 3.041(18) . ? 
Rb13 O23 3.052(16) 2_655 ? 
Rb13 O40 3.104(16) 2_655 ? 
Rb13 O46 3.264(15) 2_645 ? 
Rb13 O34 3.266(17) 2_655 ? 
Rb13 Si6 3.355(7) . ? 
Rb13 O61 3.366(15) . ? 
Rb13 Si4 3.420(7) 2_655 ? 
Rb13 O45 3.541(14) 2_655 ? 
Rb13 Rb6 3.583(4) 2_645 ? 
Rb14 O10 2.735(17) 2_645 ? 
Rb14 Si11 3.400(10) 2_655 ? 
Rb14 Si12 3.551(9) 2_645 ? 
Rb14 Rb2 3.821(4) 1_655 ? 
Rb14 Si13 4.110(8) 3_665 ? 
Rb14 Rb3 4.162(4) 2_655 ? 
Rb14 Rb5 4.242(5) 2_645 ? 
Rb14 Rb9 4.263(5) 3_665 ? 
Rb14 Rb4 4.357(5) 1_655 ? 
Rb14 Rb4 4.523(5) 3_665 ? 
Rb14 Rb2 4.527(5) 3_655 ? 
Rb14 Rb14 4.698(8) 3_765 ? 
Si1 O11 1.600(17) 2_545 ? 
Si1 O10 1.602(18) 2_545 ? 
Si1 O13 1.660(15) . ? 
Si1 O12 1.685(15) . ? 
Si1 Rb3 3.335(7) 2 ? 
Si1 Rb5 3.405(7) 2_545 ? 
Si1 Rb1 3.781(8) 2_545 ? 
Si2 O20 1.581(17) 4_576 ? 
Si2 O21 1.609(18) 4_576 ? 
Si2 O12 1.665(15) 4_566 ? 
Si2 O23 1.691(15) 4_566 ? 
Si2 Rb3 3.264(7) 3_566 ? 
Si2 Rb6 3.324(7) 4_576 ? 
Si2 Rb13 3.614(8) 3_666 ? 
Si2 Rb2 3.618(8) 4_566 ? 
Si2 Rb1 3.679(8) 3_566 ? 
Si2 Rb4 4.101(8) 4_576 ? 
Si3 O30 1.583(18) . ? 
Si3 O23 1.644(15) . ? 
Si3 O13 1.652(15) . ? 
Si3 O34 1.698(19) . ? 
Si3 Rb7 3.640(8) 4_565 ? 
Si3 Rb13 3.849(8) 2_645 ? 
Si4 O40 1.562(18) . ? 
Si4 O34 1.563(18) . ? 
Si4 O45 1.620(15) . ? 
Si4 O46 1.654(16) . ? 
Si4 Rb13 3.420(7) 2_645 ? 
Si5 O51 1.565(16) . ? 
Si5 O50 1.590(16) . ? 
Si5 O45 1.702(15) . ? 
Si5 O56 1.710(16) 2_655 ? 
Si5 Rb7 3.275(7) 3_666 ? 
Si5 Rb10 3.313(7) 2_645 ? 
Si5 Rb12 3.666(7) 2_655 ? 
Si5 Rb11 3.727(8) 2_655 ? 
Si6 O60 1.543(17) . ? 
Si6 O61 1.553(17) . ? 
Si6 O56 1.637(15) . ? 
Si6 O46 1.691(15) 2_645 ? 
Si6 Rb6 3.611(7) 2_645 ? 
Si6 Rb5 3.701(8) 2_645 ? 
Si6 Rb8 4.052(7) 2_655 ? 
Si11 Si12 2.371(12) . ? 
Si11 Si13 2.391(12) 4_566 ? 
Si11 Si14 2.445(15) . ? 
Si11 Rb14 3.400(10) 2_645 ? 
Si11 Rb2 3.599(10) 2 ? 
Si11 Rb2 3.915(12) 4_566 ? 
Si12 Si13 2.389(11) 4_566 ? 
Si12 Si14 2.396(13) . ? 
Si12 Rb14 3.551(9) 2_655 ? 
Si12 Rb9 3.552(9) 4_576 ? 
Si12 Rb12 3.823(10) 4_566 ? 
Si12 Rb2 3.894(11) 4_566 ? 
Si13 Si14 2.369(13) 4_565 ? 
Si13 Si12 2.389(11) 4_565 ? 
Si13 Si11 2.391(12) 4_565 ? 
Si13 Rb7 3.586(8) 4_565 ? 
Si13 Rb14 4.110(8) 3_665 ? 
Si14 Si13 2.369(13) 4_566 ? 
Si14 Rb9 3.692(10) 4_566 ? 
Si14 Rb12 3.738(11) 2_655 ? 
Si14 Rb12 3.761(11) 4_566 ? 
O10 Si1 1.602(18) 2 ? 
O10 Rb14 2.735(17) 2_655 ? 
O10 Rb2 2.871(17) 2 ? 
O10 Rb4 2.884(15) 2 ? 
O10 Rb3 3.121(17) 1_565 ? 
O11 Si1 1.600(17) 2 ? 
O11 Rb13 2.686(16) 2_655 ? 
O11 Rb3 3.013(17) 1_565 ? 
O11 Rb1 3.20(2) 2 ? 
O12 Si2 1.665(15) 4_565 ? 
O12 Rb1 3.238(16) 2_545 ? 
O12 Rb5 3.300(14) 2_545 ? 
O12 Rb3 3.334(15) 2_545 ? 
O20 Si2 1.581(17) 4_575 ? 
O20 Rb13 2.922(17) 2_655 ? 
O20 Rb3 2.995(16) 2 ? 
O20 Rb1 2.999(19) 2 ? 
O21 Si2 1.609(18) 4_575 ? 
O21 Rb2 2.867(17) 1_565 ? 
O21 Rb7 2.874(15) 4_575 ? 
O21 Rb3 3.207(15) 2 ? 
O23 Si2 1.691(15) 4_565 ? 
O23 Rb13 3.052(16) 2_645 ? 
O23 Rb7 3.076(17) 4_565 ? 
O23 Rb6 3.309(15) 1_545 ? 
O30 Rb7 3.11(2) 4_565 ? 
O34 Rb13 3.266(17) 2_645 ? 
O40 Rb13 3.104(16) 2_645 ? 
O45 Rb13 3.541(14) 2_645 ? 
O46 Si6 1.691(15) 2_655 ? 
O46 Rb13 3.264(15) 2_655 ? 
O50 Rb9 2.738(15) 2_645 ? 
O50 Rb10 2.990(15) 2_645 ? 
O50 Rb12 2.992(15) 2_655 ? 
O50 Rb7 3.461(17) 3_666 ? 
O51 Rb6 2.741(14) 2_645 ? 
O51 Rb10 2.941(15) 2_645 ? 
O51 Rb7 2.977(15) 3_666 ? 
O51 Rb11 3.164(15) 2_655 ? 
O56 Si5 1.710(16) 2_645 ? 
O56 Rb7 3.130(14) 4_565 ? 
O60 Rb6 2.832(15) 2_645 ? 
O60 Rb11 2.993(17) 2_655 ? 
O61 Rb8 2.800(15) 2_655 ? 
O61 Rb5 2.939(16) 2_645 ? 
 
loop_ 
 _geom_angle_atom_site_label_1 
 _geom_angle_atom_site_label_2 
 _geom_angle_atom_site_label_3 
 _geom_angle 
 _geom_angle_site_symmetry_1 
 _geom_angle_site_symmetry_3 
 _geom_angle_publ_flag 
O20 Rb1 O20 147.8(3) . 2_545 ? 
O20 Rb1 O34 97.9(5) . . ? 
O20 Rb1 O34 111.8(4) 2_545 . ? 
O20 Rb1 O11 75.8(5) . . ? 
O20 Rb1 O11 98.7(4) 2_545 . ? 
O34 Rb1 O11 120.0(4) . . ? 
O20 Rb1 O11 93.7(5) . 2_545 ? 
O20 Rb1 O11 74.0(4) 2_545 2_545 ? 
O34 Rb1 O11 91.2(4) . 2_545 ? 
O11 Rb1 O11 147.9(3) . 2_545 ? 
O20 Rb1 O13 78.7(5) . . ? 
O20 Rb1 O13 111.2(4) 2_545 . ? 
O34 Rb1 O13 49.0(4) . . ? 
O11 Rb1 O13 150.1(4) . . ? 
O11 Rb1 O13 48.6(4) 2_545 . ? 
O20 Rb1 O12 121.8(5) . 2 ? 
O20 Rb1 O12 50.1(4) 2_545 2 ? 
O34 Rb1 O12 123.9(4) . 2 ? 
O11 Rb1 O12 49.6(4) . 2 ? 
O11 Rb1 O12 120.7(4) 2_545 2 ? 
O13 Rb1 O12 159.3(4) . 2 ? 
O20 Rb1 O40 129.5(4) . . ? 
O20 Rb1 O40 81.9(4) 2_545 . ? 
O34 Rb1 O40 46.6(5) . . ? 
O11 Rb1 O40 92.1(4) . . ? 
O11 Rb1 O40 117.0(4) 2_545 . ? 
O13 Rb1 O40 92.3(4) . . ? 
O12 Rb1 O40 77.3(4) 2 . ? 
O20 Rb1 O46 84.5(4) . . ? 
O20 Rb1 O46 125.4(4) 2_545 . ? 
O34 Rb1 O46 45.1(4) . . ? 
O11 Rb1 O46 74.9(4) . . ? 
O11 Rb1 O46 135.1(4) 2_545 . ? 
O13 Rb1 O46 87.4(4) . . ? 
O12 Rb1 O46 97.3(4) 2 . ? 
O40 Rb1 O46 45.2(4) . . ? 
O20 Rb1 Si4 105.7(4) . . ? 
O20 Rb1 Si4 106.5(3) 2_545 . ? 
O34 Rb1 Si4 26.5(3) . . ? 
O11 Rb1 Si4 96.8(4) . . ? 
O11 Rb1 Si4 115.3(3) 2_545 . ? 
O13 Rb1 Si4 75.4(3) . . ? 
O12 Rb1 Si4 99.9(3) 2 . ? 
O40 Rb1 Si4 26.1(3) . . ? 
O46 Rb1 Si4 27.3(3) . . ? 
O20 Rb1 Si2 134.2(4) . 3_566 ? 
O20 Rb1 Si2 24.8(3) 2_545 3_566 ? 
O34 Rb1 Si2 126.9(4) . 3_566 ? 
O11 Rb1 Si2 74.0(3) . 3_566 ? 
O11 Rb1 Si2 94.0(3) 2_545 3_566 ? 
O13 Rb1 Si2 135.9(3) . 3_566 ? 
O12 Rb1 Si2 26.9(3) 2 3_566 ? 
O40 Rb1 Si2 85.2(3) . 3_566 ? 
O46 Rb1 Si2 118.9(3) . 3_566 ? 
Si4 Rb1 Si2 111.27(17) . 3_566 ? 
O20 Rb1 Si1 95.8(4) . 2 ? 
O20 Rb1 Si1 74.1(3) 2_545 2 ? 
O34 Rb1 Si1 131.8(3) . 2 ? 
O11 Rb1 Si1 24.7(3) . 2 ? 
O11 Rb1 Si1 133.7(3) 2_545 2 ? 
O13 Rb1 Si1 174.3(3) . 2 ? 
O12 Rb1 Si1 26.4(3) 2 2 ? 
O40 Rb1 Si1 90.4(3) . 2 ? 
O46 Rb1 Si1 91.0(3) . 2 ? 
Si4 Rb1 Si1 105.38(17) . 2 ? 
Si2 Rb1 Si1 49.31(15) 3_566 2 ? 
O21 Rb2 O10 101.8(5) 1_545 2_545 ? 
O21 Rb2 O12 52.0(4) 1_545 . ? 
O10 Rb2 O12 52.4(4) 2_545 . ? 
O21 Rb2 Si11 101.2(3) 1_545 2_545 ? 
O10 Rb2 Si11 101.3(4) 2_545 2_545 ? 
O12 Rb2 Si11 94.6(3) . 2_545 ? 
O21 Rb2 Si1 76.5(3) 1_545 . ? 
O10 Rb2 Si1 25.5(3) 2_545 . ? 
O12 Rb2 Si1 27.8(3) . . ? 
Si11 Rb2 Si1 103.9(2) 2_545 . ? 
O21 Rb2 Si2 25.5(3) 1_545 4_565 ? 
O10 Rb2 Si2 76.4(3) 2_545 4_565 ? 
O12 Rb2 Si2 27.4(3) . 4_565 ? 
Si11 Rb2 Si2 104.0(2) 2_545 4_565 ? 
Si1 Rb2 Si2 50.99(16) . 4_565 ? 
O21 Rb2 Rb7 49.3(3) 1_545 4_565 ? 
O10 Rb2 Rb7 102.2(3) 2_545 4_565 ? 
O12 Rb2 Rb7 80.5(3) . 4_565 ? 
Si11 Rb2 Rb7 145.52(17) 2_545 4_565 ? 
Si1 Rb2 Rb7 87.52(13) . 4_565 ? 
Si2 Rb2 Rb7 58.37(13) 4_565 4_565 ? 
O21 Rb2 Rb14 144.3(3) 1_545 1_455 ? 
O10 Rb2 Rb14 45.5(3) 2_545 1_455 ? 
O12 Rb2 Rb14 92.4(3) . 1_455 ? 
Si11 Rb2 Rb14 77.12(17) 2_545 1_455 ? 
Si1 Rb2 Rb14 69.60(13) . 1_455 ? 
Si2 Rb2 Rb14 119.40(14) 4_565 1_455 ? 
Rb7 Rb2 Rb14 136.81(10) 4_565 1_455 ? 
O21 Rb2 Si12 99.5(3) 1_545 4_565 ? 
O10 Rb2 Si12 129.7(3) 2_545 4_565 ? 
O12 Rb2 Si12 141.6(3) . 4_565 ? 
Si11 Rb2 Si12 118.4(2) 2_545 4_565 ? 
Si1 Rb2 Si12 137.29(18) . 4_565 ? 
Si2 Rb2 Si12 118.11(19) 4_565 4_565 ? 
Rb7 Rb2 Si12 61.22(15) 4_565 4_565 ? 
Rb14 Rb2 Si12 112.75(15) 1_455 4_565 ? 
O21 Rb2 Si13 105.2(3) 1_545 . ? 
O10 Rb2 Si13 94.4(3) 2_545 . ? 
O12 Rb2 Si13 119.0(3) . . ? 
Si11 Rb2 Si13 145.6(2) 2_545 . ? 
Si1 Rb2 Si13 103.34(18) . . ? 
Si2 Rb2 Si13 109.34(17) 4_565 . ? 
Rb7 Rb2 Si13 55.91(13) 4_565 . ? 
Rb14 Rb2 Si13 93.29(15) 1_455 . ? 
Si12 Rb2 Si13 35.73(16) 4_565 . ? 
O21 Rb2 Si11 133.6(3) 1_545 4_565 ? 
O10 Rb2 Si11 104.4(4) 2_545 4_565 ? 
O12 Rb2 Si11 149.9(3) . 4_565 ? 
Si11 Rb2 Si11 110.2(2) 2_545 4_565 ? 
Si1 Rb2 Si11 124.9(2) . 4_565 ? 
Si2 Rb2 Si11 144.72(19) 4_565 4_565 ? 
Rb7 Rb2 Si11 87.76(15) 4_565 4_565 ? 
Rb14 Rb2 Si11 77.42(16) 1_455 4_565 ? 
Si12 Rb2 Si11 35.35(18) 4_565 4_565 ? 
Si13 Rb2 Si11 35.66(18) . 4_565 ? 
O21 Rb2 Rb4 102.2(3) 1_545 . ? 
O10 Rb2 Rb4 43.9(3) 2_545 . ? 
O12 Rb2 Rb4 76.6(3) . . ? 
Si11 Rb2 Rb4 141.44(17) 2_545 . ? 
Si1 Rb2 Rb4 53.48(12) . . ? 
Si2 Rb2 Rb4 85.39(12) 4_565 . ? 
Rb7 Rb2 Rb4 70.90(7) 4_565 . ? 
Rb14 Rb2 Rb4 66.03(8) 1_455 . ? 
Si12 Rb2 Rb4 87.27(13) 4_565 . ? 
Si13 Rb2 Rb4 51.55(13) . . ? 
Si11 Rb2 Rb4 73.31(16) 4_565 . ? 
O40 Rb3 O20 93.1(5) . 2_545 ? 
O40 Rb3 O11 91.6(4) . 1_545 ? 
O20 Rb3 O11 95.5(5) 2_545 1_545 ? 
O40 Rb3 O10 134.9(4) . 1_545 ? 
O20 Rb3 O10 114.4(5) 2_545 1_545 ? 
O11 Rb3 O10 52.6(4) 1_545 1_545 ? 
O40 Rb3 O21 131.6(4) . 2_545 ? 
O20 Rb3 O21 51.5(4) 2_545 2_545 ? 
O11 Rb3 O21 119.9(4) 1_545 2_545 ? 
O10 Rb3 O21 92.8(4) 1_545 2_545 ? 
O40 Rb3 Si2 104.6(4) . 3_566 ? 
O20 Rb3 Si2 28.9(3) 2_545 3_566 ? 
O11 Rb3 Si2 120.8(4) 1_545 3_566 ? 
O10 Rb3 Si2 116.8(3) 1_545 3_566 ? 
O21 Rb3 Si2 28.8(3) 2_545 3_566 ? 
O40 Rb3 O12 84.7(4) . 2 ? 
O20 Rb3 O12 49.1(4) 2_545 2 ? 
O11 Rb3 O12 144.0(5) 1_545 2 ? 
O10 Rb3 O12 140.4(4) 1_545 2 ? 
O21 Rb3 O12 47.8(4) 2_545 2 ? 
Si2 Rb3 O12 29.2(3) 3_566 2 ? 
O40 Rb3 Si1 120.1(4) . 2_545 ? 
O20 Rb3 Si1 95.7(4) 2_545 2_545 ? 
O11 Rb3 Si1 28.6(3) 1_545 2_545 ? 
O10 Rb3 Si1 28.5(3) 1_545 2_545 ? 
O21 Rb3 Si1 97.9(3) 2_545 2_545 ? 
Si2 Rb3 Si1 110.94(18) 3_566 2_545 ? 
O12 Rb3 Si1 140.2(3) 2 2_545 ? 
O40 Rb3 Rb4 172.9(3) . 2_545 ? 
O20 Rb3 Rb4 80.2(4) 2_545 2_545 ? 
O11 Rb3 Rb4 86.8(3) 1_545 2_545 ? 
O10 Rb3 Rb4 48.0(3) 1_545 2_545 ? 
O21 Rb3 Rb4 44.8(3) 2_545 2_545 ? 
Si2 Rb3 Rb4 70.51(15) 3_566 2_545 ? 
O12 Rb3 Rb4 92.5(3) 2 2_545 ? 
Si1 Rb3 Rb4 58.90(13) 2_545 2_545 ? 
O40 Rb3 Rb5 50.5(3) . . ? 
O20 Rb3 Rb5 95.6(4) 2_545 . ? 
O11 Rb3 Rb5 141.0(3) 1_545 . ? 
O10 Rb3 Rb5 147.2(3) 1_545 . ? 
O21 Rb3 Rb5 95.9(3) 2_545 . ? 
Si2 Rb3 Rb5 83.02(14) 3_566 . ? 
O12 Rb3 Rb5 53.8(3) 2 . ? 
Si1 Rb3 Rb5 165.73(14) 2_545 . ? 
Rb4 Rb3 Rb5 131.98(9) 2_545 . ? 
O40 Rb3 Si11 98.0(4) . . ? 
O20 Rb3 Si11 132.3(4) 2_545 . ? 
O11 Rb3 Si11 130.1(4) 1_545 . ? 
O10 Rb3 Si11 89.2(3) 1_545 . ? 
O21 Rb3 Si11 88.6(3) 2_545 . ? 
Si2 Rb3 Si11 103.9(2) 3_566 . ? 
O12 Rb3 Si11 85.8(3) 2 . ? 
Si1 Rb3 Si11 117.3(2) 2_545 . ? 
Rb4 Rb3 Si11 88.27(18) 2_545 . ? 
Rb5 Rb3 Si11 59.55(16) . . ? 
O40 Rb3 Rb8 47.0(3) . . ? 
O20 Rb3 Rb8 139.0(4) 2_545 . ? 
O11 Rb3 Rb8 79.3(3) 1_545 . ? 
O10 Rb3 Rb8 94.7(3) 1_545 . ? 
O21 Rb3 Rb8 159.6(3) 2_545 . ? 
Si2 Rb3 Rb8 148.37(15) 3_566 . ? 
O12 Rb3 Rb8 120.8(3) 2 . ? 
Si1 Rb3 Rb8 97.78(13) 2_545 . ? 
Rb4 Rb3 Rb8 139.06(9) 2_545 . ? 
Rb5 Rb3 Rb8 67.96(7) . . ? 
Si11 Rb3 Rb8 72.64(17) . . ? 
O21 Rb4 O10 109.5(5) . 2_545 ? 
O21 Rb4 O13 95.1(5) . . ? 
O10 Rb4 O13 54.4(4) 2_545 . ? 
O21 Rb4 O30 106.4(5) . . ? 
O10 Rb4 O30 99.1(4) 2_545 . ? 
O13 Rb4 O30 52.4(4) . . ? 
O21 Rb4 Si13 142.9(4) . . ? 
O10 Rb4 Si13 102.9(4) 2_545 . ? 
O13 Rb4 Si13 118.7(3) . . ? 
O30 Rb4 Si13 85.3(4) . . ? 
O21 Rb4 Si1 103.3(4) . . ? 
O10 Rb4 Si1 26.6(3) 2_545 . ? 
O13 Rb4 Si1 27.9(3) . . ? 
O30 Rb4 Si1 76.2(3) . . ? 
Si13 Rb4 Si1 113.65(18) . . ? 
O21 Rb4 Si3 104.1(4) . . ? 
O10 Rb4 Si3 75.6(3) 2_545 . ? 
O13 Rb4 Si3 26.7(3) . . ? 
O30 Rb4 Si3 25.9(3) . . ? 
Si13 Rb4 Si3 100.89(18) . . ? 
Si1 Rb4 Si3 50.86(15) . . ? 
O21 Rb4 Rb6 57.1(4) . . ? 
O10 Rb4 Rb6 115.8(4) 2_545 . ? 
O13 Rb4 Rb6 64.3(3) . . ? 
O30 Rb4 Rb6 49.3(4) . . ? 
Si13 Rb4 Rb6 122.48(15) . . ? 
Si1 Rb4 Rb6 90.46(14) . . ? 
Si3 Rb4 Rb6 54.74(12) . . ? 
O21 Rb4 Rb3 56.0(3) . 2 ? 
O10 Rb4 Rb3 53.6(3) 2_545 2 ? 
O13 Rb4 Rb3 64.3(3) . 2 ? 
O30 Rb4 Rb3 112.5(3) . 2 ? 
Si13 Rb4 Rb3 151.15(15) . 2 ? 
Si1 Rb4 Rb3 53.96(12) . 2 ? 
Si3 Rb4 Rb3 89.56(13) . 2 ? 
Rb6 Rb4 Rb3 85.51(8) . 2 ? 
O21 Rb4 Rb10 103.6(3) . . ? 
O10 Rb4 Rb10 135.9(3) 2_545 . ? 
O13 Rb4 Rb10 95.1(3) . . ? 
O30 Rb4 Rb10 42.7(3) . . ? 
Si13 Rb4 Rb10 61.32(14) . . ? 
Si1 Rb4 Rb10 117.86(13) . . ? 
Si3 Rb4 Rb10 68.63(12) . . ? 
Rb6 Rb4 Rb10 61.23(7) . . ? 
Rb3 Rb4 Rb10 146.48(10) 2 . ? 
O21 Rb4 Si2 14.4(4) . 4_575 ? 
O10 Rb4 Si2 100.8(4) 2_545 4_575 ? 
O13 Rb4 Si2 80.7(3) . 4_575 ? 
O30 Rb4 Si2 97.2(4) . 4_575 ? 
Si13 Rb4 Si2 155.47(18) . 4_575 ? 
Si1 Rb4 Si2 90.53(16) . 4_575 ? 
Si3 Rb4 Si2 91.08(16) . 4_575 ? 
Rb6 Rb4 Si2 49.63(11) . 4_575 ? 
Rb3 Rb4 Si2 48.61(11) 2 4_575 ? 
Rb10 Rb4 Si2 104.67(12) . 4_575 ? 
O21 Rb4 Rb2 152.8(3) . . ? 
O10 Rb4 Rb2 43.6(3) 2_545 . ? 
O13 Rb4 Rb2 73.1(3) . . ? 
O30 Rb4 Rb2 86.1(4) . . ? 
Si13 Rb4 Rb2 60.35(14) . . ? 
Si1 Rb4 Rb2 55.35(12) . . ? 
Si3 Rb4 Rb2 76.42(12) . . ? 
Rb6 Rb4 Rb2 131.12(9) . . ? 
Rb3 Rb4 Rb2 97.01(8) 2 . ? 
Rb10 Rb4 Rb2 101.85(8) . . ? 
Si2 Rb4 Rb2 144.03(13) 4_575 . ? 
O61 Rb5 O40 96.1(5) 2_655 . ? 
O61 Rb5 O11 90.1(4) 2_655 . ? 
O40 Rb5 O11 100.3(4) . . ? 
O61 Rb5 O46 50.4(4) 2_655 . ? 
O40 Rb5 O46 50.6(4) . . ? 
O11 Rb5 O46 80.1(4) . . ? 
O61 Rb5 O12 137.5(4) 2_655 2 ? 
O40 Rb5 O12 81.8(4) . 2 ? 
O11 Rb5 O12 49.3(4) . 2 ? 
O46 Rb5 O12 102.6(4) . 2 ? 
O61 Rb5 Si1 116.4(3) 2_655 2 ? 
O40 Rb5 Si1 104.9(3) . 2 ? 
O11 Rb5 Si1 27.9(3) . 2 ? 
O46 Rb5 Si1 104.1(3) . 2 ? 
O12 Rb5 Si1 29.1(3) 2 2 ? 
O61 Rb5 O10 119.2(4) 2_655 . ? 
O40 Rb5 O10 128.0(4) . . ? 
O11 Rb5 O10 47.9(4) . . ? 
O46 Rb5 O10 128.0(4) . . ? 
O12 Rb5 O10 46.2(4) 2 . ? 
Si1 Rb5 O10 26.8(3) 2 . ? 
O61 Rb5 Si4 72.5(3) 2_655 . ? 
O40 Rb5 Si4 24.4(3) . . ? 
O11 Rb5 Si4 94.0(3) . . ? 
O46 Rb5 Si4 26.6(3) . . ? 
O12 Rb5 Si4 95.3(3) 2 . ? 
Si1 Rb5 Si4 109.77(18) 2 . ? 
O10 Rb5 Si4 136.5(3) . . ? 
O61 Rb5 Si6 23.7(3) 2_655 2_655 ? 
O40 Rb5 Si6 73.2(3) . 2_655 ? 
O11 Rb5 Si6 88.2(3) . 2_655 ? 
O46 Rb5 Si6 27.1(3) . 2_655 ? 
O12 Rb5 Si6 125.5(3) 2 2_655 ? 
Si1 Rb5 Si6 116.04(18) 2 2_655 ? 
O10 Rb5 Si6 130.5(3) . 2_655 ? 
Si4 Rb5 Si6 49.13(14) . 2_655 ? 
O61 Rb5 Rb3 141.3(3) 2_655 . ? 
O40 Rb5 Rb3 45.4(3) . . ? 
O11 Rb5 Rb3 99.4(3) . . ? 
O46 Rb5 Rb3 94.2(3) . . ? 
O12 Rb5 Rb3 54.7(3) 2 . ? 
Si1 Rb5 Rb3 83.69(13) 2 . ? 
O10 Rb5 Rb3 93.8(3) . . ? 
Si4 Rb5 Rb3 69.52(12) . . ? 
Si6 Rb5 Rb3 118.60(12) 2_655 . ? 
O61 Rb5 Si11 135.0(3) 2_655 . ? 
O40 Rb5 Si11 95.3(4) . . ? 
O11 Rb5 Si11 130.1(3) . . ? 
O46 Rb5 Si11 141.2(3) . . ? 
O12 Rb5 Si11 87.3(3) 2 . ? 
Si1 Rb5 Si11 102.2(2) 2 . ? 
O10 Rb5 Si11 85.7(3) . . ? 
Si4 Rb5 Si11 116.3(2) . . ? 
Si6 Rb5 Si11 141.6(2) 2_655 . ? 
Rb3 Rb5 Si11 61.05(15) . . ? 
O61 Rb5 Si14 100.5(3) 2_655 . ? 
O40 Rb5 Si14 88.9(3) . . ? 
O11 Rb5 Si14 165.2(3) . . ? 
O46 Rb5 Si14 114.6(3) . . ? 
O12 Rb5 Si14 121.8(3) 2 . ? 
Si1 Rb5 Si14 138.3(2) 2 . ? 
O10 Rb5 Si14 117.4(3) . . ? 
Si4 Rb5 Si14 98.96(18) . . ? 
Si6 Rb5 Si14 105.6(2) 2_655 . ? 
Rb3 Rb5 Si14 78.68(17) . . ? 
Si11 Rb5 Si14 36.5(2) . . ? 
O51 Rb6 O60 83.2(5) 2_655 2_655 ? 
O51 Rb6 O30 90.8(4) 2_655 . ? 
O60 Rb6 O30 124.0(5) 2_655 . ? 
O51 Rb6 O46 127.6(4) 2_655 . ? 
O60 Rb6 O46 51.5(4) 2_655 . ? 
O30 Rb6 O46 94.3(5) . . ? 
O51 Rb6 O20 135.0(4) 2_655 . ? 
O60 Rb6 O20 106.0(5) 2_655 . ? 
O30 Rb6 O20 116.4(5) . . ? 
O46 Rb6 O20 87.6(4) . . ? 
O51 Rb6 O21 92.5(4) 2_655 . ? 
O60 Rb6 O21 135.6(4) 2_655 . ? 
O30 Rb6 O21 100.2(5) . . ? 
O46 Rb6 O21 137.2(4) . . ? 
O20 Rb6 O21 49.9(4) . . ? 
O51 Rb6 O34 132.9(4) 2_655 . ? 
O60 Rb6 O34 95.9(5) 2_655 . ? 
O30 Rb6 O34 51.1(5) . . ? 
O46 Rb6 O34 47.7(4) . . ? 
O20 Rb6 O34 90.7(4) . . ? 
O21 Rb6 O34 117.8(4) . . ? 
O51 Rb6 O23 89.1(4) 2_655 1_565 ? 
O60 Rb6 O23 87.3(4) 2_655 1_565 ? 
O30 Rb6 O23 148.5(5) . 1_565 ? 
O46 Rb6 O23 110.4(4) . 1_565 ? 
O20 Rb6 O23 48.7(4) . 1_565 ? 
O21 Rb6 O23 48.4(4) . 1_565 ? 
O34 Rb6 O23 137.9(4) . 1_565 ? 
O51 Rb6 Si2 107.2(3) 2_655 4_575 ? 
O60 Rb6 Si2 112.1(4) 2_655 4_575 ? 
O30 Rb6 Si2 122.8(4) . 4_575 ? 
O46 Rb6 Si2 113.1(3) . 4_575 ? 
O20 Rb6 Si2 28.1(3) . 4_575 ? 
O21 Rb6 Si2 28.3(3) . 4_575 ? 
O34 Rb6 Si2 116.3(3) . 4_575 ? 
O23 Rb6 Si2 29.5(3) 1_565 4_575 ? 
O51 Rb6 Si3 118.5(3) 2_655 . ? 
O60 Rb6 Si3 122.6(4) 2_655 . ? 
O30 Rb6 Si3 27.6(3) . . ? 
O46 Rb6 Si3 77.1(3) . . ? 
O20 Rb6 Si3 93.8(3) . . ? 
O21 Rb6 Si3 98.2(3) . . ? 
O34 Rb6 Si3 29.4(3) . . ? 
O23 Rb6 Si3 139.6(3) 1_565 . ? 
Si2 Rb6 Si3 110.17(17) 4_575 . ? 
O51 Rb6 Rb13 119.9(3) 2_655 2_655 ? 
O60 Rb6 Rb13 55.1(4) 2_655 2_655 ? 
O30 Rb6 Rb13 146.8(3) . 2_655 ? 
O46 Rb6 Rb13 58.0(3) . 2_655 ? 
O20 Rb6 Rb13 50.9(3) . 2_655 ? 
O21 Rb6 Rb13 91.2(3) . 2_655 ? 
O34 Rb6 Rb13 96.0(3) . 2_655 ? 
O23 Rb6 Rb13 52.4(3) 1_565 2_655 ? 
Si2 Rb6 Rb13 62.97(14) 4_575 2_655 ? 
Si3 Rb6 Rb13 120.17(15) . 2_655 ? 
O51 Rb6 Si6 102.5(3) 2_655 2_655 ? 
O60 Rb6 Si6 24.0(3) 2_655 2_655 ? 
O30 Rb6 Si6 109.0(4) . 2_655 ? 
O46 Rb6 Si6 27.9(3) . 2_655 ? 
O20 Rb6 Si6 101.3(3) . 2_655 ? 
O21 Rb6 Si6 146.8(3) . 2_655 ? 
O34 Rb6 Si6 72.3(3) . 2_655 ? 
O23 Rb6 Si6 101.7(3) 1_565 2_655 ? 
Si2 Rb6 Si6 118.55(19) 4_575 2_655 ? 
Si3 Rb6 Si6 100.26(17) . 2_655 ? 
Rb13 Rb6 Si6 55.58(12) 2_655 2_655 ? 
O21 Rb7 O51 95.8(4) 4_576 3_666 ? 
O21 Rb7 O23 53.6(4) 4_576 4_566 ? 
O51 Rb7 O23 89.6(4) 3_666 4_566 ? 
O21 Rb7 O30 100.6(5) 4_576 4_566 ? 
O51 Rb7 O30 105.0(5) 3_666 4_566 ? 
O23 Rb7 O30 51.1(4) 4_566 4_566 ? 
O21 Rb7 O56 147.7(4) 4_576 4_566 ? 
O51 Rb7 O56 52.6(4) 3_666 4_566 ? 
O23 Rb7 O56 112.6(4) 4_566 4_566 ? 
O30 Rb7 O56 83.9(4) 4_566 4_566 ? 
O21 Rb7 Si5 121.6(3) 4_576 3_666 ? 
O51 Rb7 Si5 28.5(3) 3_666 3_666 ? 
O23 Rb7 Si5 114.0(3) 4_566 3_666 ? 
O30 Rb7 Si5 108.4(4) 4_566 3_666 ? 
O56 Rb7 Si5 30.9(3) 4_566 3_666 ? 
O21 Rb7 O50 118.5(4) 4_576 3_666 ? 
O51 Rb7 O50 47.6(4) 3_666 3_666 ? 
O23 Rb7 O50 137.0(4) 4_566 3_666 ? 
O30 Rb7 O50 131.7(4) 4_566 3_666 ? 
O56 Rb7 O50 47.8(4) 4_566 3_666 ? 
Si5 Rb7 O50 27.1(3) 3_666 3_666 ? 
O21 Rb7 Si13 113.2(4) 4_576 4_566 ? 
O51 Rb7 Si13 146.9(3) 3_666 4_566 ? 
O23 Rb7 Si13 120.1(3) 4_566 4_566 ? 
O30 Rb7 Si13 85.7(4) 4_566 4_566 ? 
O56 Rb7 Si13 99.0(3) 4_566 4_566 ? 
Si5 Rb7 Si13 118.4(2) 3_666 4_566 ? 
O50 Rb7 Si13 102.0(3) 3_666 4_566 ? 
O21 Rb7 Si2 25.9(3) 4_576 . ? 
O51 Rb7 Si2 95.8(3) 3_666 . ? 
O23 Rb7 Si2 28.0(3) 4_566 . ? 
O30 Rb7 Si2 75.7(3) 4_566 . ? 
O56 Rb7 Si2 136.2(3) 4_566 . ? 
Si5 Rb7 Si2 124.28(18) 3_666 . ? 
O50 Rb7 Si2 134.7(3) 3_666 . ? 
Si13 Rb7 Si2 117.29(19) 4_566 . ? 
O21 Rb7 Si3 75.3(3) 4_576 4_566 ? 
O51 Rb7 Si3 103.6(3) 3_666 4_566 ? 
O23 Rb7 Si3 26.7(3) 4_566 4_566 ? 
O30 Rb7 Si3 25.6(3) 4_566 4_566 ? 
O56 Rb7 Si3 103.2(3) 4_566 4_566 ? 
Si5 Rb7 Si3 119.27(18) 3_666 4_566 ? 
O50 Rb7 Si3 146.4(3) 3_666 4_566 ? 
Si13 Rb7 Si3 99.13(19) 4_566 4_566 ? 
Si2 Rb7 Si3 50.04(15) . 4_566 ? 
O21 Rb7 Rb2 49.1(3) 4_576 4_566 ? 
O51 Rb7 Rb2 142.7(3) 3_666 4_566 ? 
O23 Rb7 Rb2 79.1(3) 4_566 4_566 ? 
O30 Rb7 Rb2 95.2(4) 4_566 4_566 ? 
O56 Rb7 Rb2 163.0(3) 4_566 4_566 ? 
Si5 Rb7 Rb2 156.26(15) 3_666 4_566 ? 
O50 Rb7 Rb2 131.3(3) 3_666 4_566 ? 
Si13 Rb7 Rb2 64.10(14) 4_566 4_566 ? 
Si2 Rb7 Rb2 58.99(13) . 4_566 ? 
Si3 Rb7 Rb2 81.66(13) 4_566 4_566 ? 
O21 Rb7 Rb11 105.0(4) 4_576 4_566 ? 
O51 Rb7 Rb11 53.0(3) 3_666 4_566 ? 
O23 Rb7 Rb11 59.6(3) 4_566 4_566 ? 
O30 Rb7 Rb11 52.1(4) 4_566 4_566 ? 
O56 Rb7 Rb11 53.0(3) 4_566 4_566 ? 
Si5 Rb7 Rb11 62.11(14) 3_666 4_566 ? 
O50 Rb7 Rb11 89.2(3) 3_666 4_566 ? 
Si13 Rb7 Rb11 127.50(15) 4_566 4_566 ? 
Si2 Rb7 Rb11 84.35(13) . 4_566 ? 
Si3 Rb7 Rb11 57.16(12) 4_566 4_566 ? 
Rb2 Rb7 Rb11 137.51(9) 4_566 4_566 ? 
O61 Rb8 O50 104.0(5) 2_645 . ? 
O61 Rb8 O40 116.0(5) 2_645 . ? 
O50 Rb8 O40 98.2(4) . . ? 
O61 Rb8 O45 96.9(4) 2_645 . ? 
O50 Rb8 O45 54.3(4) . . ? 
O40 Rb8 O45 52.7(4) . . ? 
O61 Rb8 Si14 138.4(4) 2_645 . ? 
O50 Rb8 Si14 90.2(4) . . ? 
O40 Rb8 Si14 99.9(4) . . ? 
O45 Rb8 Si14 122.4(3) . . ? 
O61 Rb8 Si4 110.1(4) 2_645 . ? 
O50 Rb8 Si4 75.4(3) . . ? 
O40 Rb8 Si4 25.7(3) . . ? 
O45 Rb8 Si4 27.1(3) . . ? 
Si14 Rb8 Si4 111.4(2) . . ? 
O61 Rb8 Si5 102.3(4) 2_645 . ? 
O50 Rb8 Si5 25.9(3) . . ? 
O40 Rb8 Si5 75.8(4) . . ? 
O45 Rb8 Si5 28.5(3) . . ? 
Si14 Rb8 Si5 106.5(2) . . ? 
Si4 Rb8 Si5 51.09(15) . . ? 
O61 Rb8 Rb13 61.1(3) 2_645 2_645 ? 
O50 Rb8 Rb13 113.1(3) . 2_645 ? 
O40 Rb8 Rb13 54.9(3) . 2_645 ? 
O45 Rb8 Rb13 63.1(3) . 2_645 ? 
Si14 Rb8 Rb13 146.6(2) . 2_645 ? 
Si4 Rb8 Rb13 56.67(12) . 2_645 ? 
Si5 Rb8 Rb13 89.45(13) . 2_645 ? 
O61 Rb8 Rb10 55.2(3) 2_645 2_645 ? 
O50 Rb8 Rb10 48.9(3) . 2_645 ? 
O40 Rb8 Rb10 114.8(4) . 2_645 ? 
O45 Rb8 Rb10 64.0(3) . 2_645 ? 
Si14 Rb8 Rb10 127.7(2) . 2_645 ? 
Si4 Rb8 Rb10 90.51(13) . 2_645 ? 
Si5 Rb8 Rb10 52.00(11) . 2_645 ? 
Rb13 Rb8 Rb10 85.30(8) 2_645 2_645 ? 
O61 Rb8 Rb3 108.0(3) 2_645 . ? 
O50 Rb8 Rb3 138.7(3) . . ? 
O40 Rb8 Rb3 44.1(3) . . ? 
O45 Rb8 Rb3 96.1(3) . . ? 
Si14 Rb8 Rb3 82.93(19) . . ? 
Si4 Rb8 Rb3 69.63(12) . . ? 
Si5 Rb8 Rb3 119.61(13) . . ? 
Rb13 Rb8 Rb3 63.70(7) 2_645 . ? 
Rb10 Rb8 Rb3 148.71(9) 2_645 . ? 
O61 Rb8 Rb9 97.2(3) 2_645 2_645 ? 
O50 Rb8 Rb9 42.5(3) . 2_645 ? 
O40 Rb8 Rb9 135.4(3) . 2_645 ? 
O45 Rb8 Rb9 96.7(3) . 2_645 ? 
Si14 Rb8 Rb9 67.35(19) . 2_645 ? 
Si4 Rb8 Rb9 116.88(13) . 2_645 ? 
Si5 Rb8 Rb9 68.32(13) . 2_645 ? 
Rb13 Rb8 Rb9 145.67(10) 2_645 2_645 ? 
Rb10 Rb8 Rb9 60.45(8) 2_645 2_645 ? 
Rb3 Rb8 Rb9 150.04(9) . 2_645 ? 
O61 Rb8 Si6 15.7(3) 2_645 2_645 ? 
O50 Rb8 Si6 96.2(3) . 2_645 ? 
O40 Rb8 Si6 104.5(3) . 2_645 ? 
O45 Rb8 Si6 81.3(3) . 2_645 ? 
Si14 Rb8 Si6 153.6(2) . 2_645 ? 
Si4 Rb8 Si6 95.05(16) . 2_645 ? 
Si5 Rb8 Si6 89.41(15) . 2_645 ? 
Rb13 Rb8 Si6 51.26(11) 2_645 2_645 ? 
Rb10 Rb8 Si6 48.27(10) 2_645 2_645 ? 
Rb3 Rb8 Si6 107.82(11) . 2_645 ? 
Rb9 Rb8 Si6 100.85(12) 2_645 2_645 ? 
O50 Rb9 Si12 96.8(4) 2_655 4_575 ? 
O50 Rb9 Si13 107.1(3) 2_655 . ? 
Si12 Rb9 Si13 111.0(2) 4_575 . ? 
O50 Rb9 Si14 136.0(4) 2_655 4_565 ? 
Si12 Rb9 Si14 118.1(2) 4_575 4_565 ? 
Si13 Rb9 Si14 37.7(2) . 4_565 ? 
O50 Rb9 Rb12 52.9(3) 2_655 1_565 ? 
Si12 Rb9 Rb12 63.62(16) 4_575 1_565 ? 
Si13 Rb9 Rb12 155.54(16) . 1_565 ? 
Si14 Rb9 Rb12 166.73(18) 4_565 1_565 ? 
O50 Rb9 Rb10 47.9(3) 2_655 . ? 
Si12 Rb9 Rb10 120.60(18) 4_575 . ? 
Si13 Rb9 Rb10 60.11(13) . . ? 
Si14 Rb9 Rb10 89.56(17) 4_565 . ? 
Rb12 Rb9 Rb10 100.71(9) 1_565 . ? 
O50 Rb9 Rb8 45.2(3) 2_655 2_655 ? 
Si12 Rb9 Rb8 133.65(16) 4_575 2_655 ? 
Si13 Rb9 Rb8 106.11(15) . 2_655 ? 
Si14 Rb9 Rb8 108.22(19) 4_565 2_655 ? 
Rb12 Rb9 Rb8 71.01(7) 1_565 2_655 ? 
Rb10 Rb9 Rb8 58.60(7) . 2_655 ? 
O50 Rb9 Rb14 129.2(4) 2_655 3_665 ? 
Si12 Rb9 Rb14 53.10(15) 4_575 3_665 ? 
Si13 Rb9 Rb14 62.10(14) . 3_665 ? 
Si14 Rb9 Rb14 67.01(19) 4_565 3_665 ? 
Rb12 Rb9 Rb14 116.68(9) 1_565 3_665 ? 
Rb10 Rb9 Rb14 108.18(9) . 3_665 ? 
Rb8 Rb9 Rb14 166.56(10) 2_655 3_665 ? 
O50 Rb9 Rb9 114.1(4) 2_655 3_665 ? 
Si12 Rb9 Rb9 132.2(2) 4_575 3_665 ? 
Si13 Rb9 Rb9 94.28(16) . 3_665 ? 
Si14 Rb9 Rb9 61.86(18) 4_565 3_665 ? 
Rb12 Rb9 Rb9 106.62(11) 1_565 3_665 ? 
Rb10 Rb9 Rb9 107.09(10) . 3_665 ? 
Rb8 Rb9 Rb9 69.21(9) 2_655 3_665 ? 
Rb14 Rb9 Rb9 116.11(11) 3_665 3_665 ? 
O50 Rb9 Rb12 113.0(3) 2_655 3_665 ? 
Si12 Rb9 Rb12 66.93(17) 4_575 3_665 ? 
Si13 Rb9 Rb12 139.84(15) . 3_665 ? 
Si14 Rb9 Rb12 105.32(17) 4_565 3_665 ? 
Rb12 Rb9 Rb12 62.49(8) 1_565 3_665 ? 
Rb10 Rb9 Rb12 157.83(9) . 3_665 ? 
Rb8 Rb9 Rb12 100.49(9) 2_655 3_665 ? 
Rb14 Rb9 Rb12 92.93(8) 3_665 3_665 ? 
Rb9 Rb9 Rb12 67.70(9) 3_665 3_665 ? 
O50 Rb9 Rb7 48.1(3) 2_655 4_575 ? 
Si12 Rb9 Rb7 54.96(16) 4_575 4_575 ? 
Si13 Rb9 Rb7 98.91(16) . 4_575 ? 
Si14 Rb9 Rb7 134.91(18) 4_565 4_575 ? 
Rb12 Rb9 Rb7 57.78(7) 1_565 4_575 ? 
Rb10 Rb9 Rb7 68.10(7) . 4_575 ? 
Rb8 Rb9 Rb7 93.19(8) 2_655 4_575 ? 
Rb14 Rb9 Rb7 82.95(8) 3_665 4_575 ? 
Rb9 Rb9 Rb7 160.47(11) 3_665 4_575 ? 
Rb12 Rb9 Rb7 109.18(8) 3_665 4_575 ? 
O50 Rb9 Rb8 165.4(4) 2_655 4_565 ? 
Si12 Rb9 Rb8 91.85(16) 4_575 4_565 ? 
Si13 Rb9 Rb8 80.46(14) . 4_565 ? 
Si14 Rb9 Rb8 45.98(15) 4_565 4_565 ? 
Rb12 Rb9 Rb8 122.42(9) 1_565 4_565 ? 
Rb10 Rb9 Rb8 135.08(8) . 4_565 ? 
Rb8 Rb9 Rb8 121.26(8) 2_655 4_565 ? 
Rb14 Rb9 Rb8 65.29(7) 3_665 4_565 ? 
Rb9 Rb9 Rb8 52.05(7) 3_665 4_565 ? 
Rb12 Rb9 Rb8 59.96(6) 3_665 4_565 ? 
Rb7 Rb9 Rb8 144.56(8) 4_575 4_565 ? 
O30 Rb10 O51 91.7(5) . 2_655 ? 
O30 Rb10 O50 137.4(5) . 2_655 ? 
O51 Rb10 O50 52.7(4) 2_655 2_655 ? 
O30 Rb10 O60 95.0(5) . . ? 
O51 Rb10 O60 96.0(4) 2_655 . ? 
O50 Rb10 O60 109.8(5) 2_655 . ? 
O30 Rb10 Si6 105.5(4) . . ? 
O51 Rb10 Si6 120.8(3) 2_655 . ? 
O50 Rb10 Si6 112.6(3) 2_655 . ? 
O60 Rb10 Si6 28.1(3) . . ? 
O30 Rb10 O61 131.0(5) . . ? 
O51 Rb10 O61 120.5(4) 2_655 . ? 
O50 Rb10 O61 90.6(4) 2_655 . ? 
O60 Rb10 O61 49.5(4) . . ? 
Si6 Rb10 O61 27.4(3) . . ? 
O30 Rb10 Si5 119.9(5) . 2_655 ? 
O51 Rb10 Si5 28.2(3) 2_655 2_655 ? 
O50 Rb10 Si5 28.6(3) 2_655 2_655 ? 
O60 Rb10 Si5 93.7(4) . 2_655 ? 
Si6 Rb10 Si5 109.20(17) . 2_655 ? 
O61 Rb10 Si5 97.9(3) . 2_655 ? 
O30 Rb10 O56 85.6(5) . . ? 
O51 Rb10 O56 143.2(4) 2_655 . ? 
O50 Rb10 O56 136.6(4) 2_655 . ? 
O60 Rb10 O56 47.9(4) . . ? 
Si6 Rb10 O56 28.5(3) . . ? 
O61 Rb10 O56 46.1(4) . . ? 
Si5 Rb10 O56 137.6(3) 2_655 . ? 
O30 Rb10 Si13 86.1(5) . . ? 
O51 Rb10 Si13 126.6(3) 2_655 . ? 
O50 Rb10 Si13 97.0(3) 2_655 . ? 
O60 Rb10 Si13 137.3(3) . . ? 
Si6 Rb10 Si13 110.97(18) . . ? 
O61 Rb10 Si13 99.4(3) . . ? 
Si5 Rb10 Si13 122.55(17) 2_655 . ? 
O56 Rb10 Si13 89.8(3) . . ? 
O30 Rb10 Rb7 52.7(4) . 4_565 ? 
O51 Rb10 Rb7 144.2(3) 2_655 4_565 ? 
O50 Rb10 Rb7 152.0(3) 2_655 4_565 ? 
O60 Rb10 Rb7 92.3(3) . 4_565 ? 
Si6 Rb10 Rb7 78.96(13) . 4_565 ? 
O61 Rb10 Rb7 91.1(3) . 4_565 ? 
Si5 Rb10 Rb7 171.04(15) 2_655 4_565 ? 
O56 Rb10 Rb7 50.5(2) . 4_565 ? 
Si13 Rb10 Rb7 55.21(12) . 4_565 ? 
O30 Rb10 Rb11 82.4(5) . 2_655 ? 
O51 Rb10 Rb11 49.2(3) 2_655 2_655 ? 
O50 Rb10 Rb11 88.2(3) 2_655 2_655 ? 
O60 Rb10 Rb11 49.3(3) . 2_655 ? 
Si6 Rb10 Rb11 77.08(14) . 2_655 ? 
O61 Rb10 Rb11 91.9(3) . 2_655 ? 
Si5 Rb10 Rb11 60.46(13) 2_655 2_655 ? 
O56 Rb10 Rb11 94.2(2) . 2_655 ? 
Si13 Rb10 Rb11 167.47(15) . 2_655 ? 
Rb7 Rb10 Rb11 119.63(8) 4_565 2_655 ? 
O30 Rb10 Rb8 169.2(4) . 2_655 ? 
O51 Rb10 Rb8 85.4(3) 2_655 2_655 ? 
O50 Rb10 Rb8 46.4(3) 2_655 2_655 ? 
O60 Rb10 Rb8 75.0(4) . 2_655 ? 
Si6 Rb10 Rb8 67.47(14) . 2_655 ? 
O61 Rb10 Rb8 44.3(3) . 2_655 ? 
Si5 Rb10 Rb8 57.97(14) 2_655 2_655 ? 
O56 Rb10 Rb8 90.4(3) . 2_655 ? 
Si13 Rb10 Rb8 103.89(15) . 2_655 ? 
Rb7 Rb10 Rb8 130.33(9) 4_565 2_655 ? 
Rb11 Rb10 Rb8 87.97(8) 2_655 2_655 ? 
O51 Rb11 O60 95.3(4) . 2_645 ? 
O51 Rb11 O45 52.1(4) . . ? 
O60 Rb11 O45 78.1(4) 2_645 . ? 
O51 Rb11 O30 112.8(5) . . ? 
O60 Rb11 O30 126.9(5) 2_645 . ? 
O45 Rb11 O30 85.0(5) . . ? 
O51 Rb11 O60 74.3(4) . . ? 
O60 Rb11 O60 148.1(3) 2_645 . ? 
O45 Rb11 O60 114.6(4) . . ? 
O30 Rb11 O60 84.4(4) . . ? 
O51 Rb11 O51 144.6(3) . 2_645 ? 
O60 Rb11 O51 73.8(4) 2_645 2_645 ? 
O45 Rb11 O51 148.2(4) . 2_645 ? 
O30 Rb11 O51 100.0(5) . 2_645 ? 
O60 Rb11 O51 97.1(4) . 2_645 ? 
O51 Rb11 O56 119.8(4) . . ? 
O60 Rb11 O56 122.0(4) 2_645 . ? 
O45 Rb11 O56 159.8(4) . . ? 
O30 Rb11 O56 82.3(4) . . ? 
O60 Rb11 O56 48.6(4) . . ? 
O51 Rb11 O56 50.4(4) 2_645 . ? 
O51 Rb11 O23 133.5(4) . . ? 
O60 Rb11 O23 81.0(4) 2_645 . ? 
O45 Rb11 O23 82.2(4) . . ? 
O30 Rb11 O23 46.8(4) . . ? 
O60 Rb11 O23 128.2(4) . . ? 
O51 Rb11 O23 79.0(4) 2_645 . ? 
O56 Rb11 O23 100.2(4) . . ? 
O51 Rb11 Si3 114.6(3) . . ? 
O60 Rb11 Si3 101.8(4) 2_645 . ? 
O45 Rb11 Si3 70.7(3) . . ? 
O30 Rb11 Si3 26.0(3) . . ? 
O60 Rb11 Si3 110.0(3) . . ? 
O51 Rb11 Si3 100.7(3) 2_645 . ? 
O56 Rb11 Si3 102.6(3) . . ? 
O23 Rb11 Si3 26.6(3) . . ? 
O51 Rb11 Si5 24.6(3) . . ? 
O60 Rb11 Si5 86.9(3) 2_645 . ? 
O45 Rb11 Si5 27.5(3) . . ? 
O30 Rb11 Si5 100.4(4) . . ? 
O60 Rb11 Si5 93.5(3) . . ? 
O51 Rb11 Si5 157.7(3) 2_645 . ? 
O56 Rb11 Si5 141.8(3) . . ? 
O23 Rb11 Si5 109.4(3) . . ? 
Si3 Rb11 Si5 93.97(16) . . ? 
O51 Rb11 Si5 131.8(3) . 2_645 ? 
O60 Rb11 Si5 94.9(4) 2_645 2_645 ? 
O45 Rb11 Si5 172.7(3) . 2_645 ? 
O30 Rb11 Si5 97.6(4) . 2_645 ? 
O60 Rb11 Si5 72.5(3) . 2_645 ? 
O51 Rb11 Si5 24.6(3) 2_645 2_645 ? 
O56 Rb11 Si5 27.2(3) . 2_645 ? 
O23 Rb11 Si5 94.6(3) . 2_645 ? 
Si3 Rb11 Si5 109.04(17) . 2_645 ? 
Si5 Rb11 Si5 155.95(8) . 2_645 ? 
O51 Rb11 Si6 94.6(3) . . ? 
O60 Rb11 Si6 135.9(4) 2_645 . ? 
O45 Rb11 Si6 138.4(3) . . ? 
O30 Rb11 Si6 87.4(3) . . ? 
O60 Rb11 Si6 23.8(3) . . ? 
O51 Rb11 Si6 73.4(3) 2_645 . ? 
O56 Rb11 Si6 25.6(3) . . ? 
O23 Rb11 Si6 120.1(3) . . ? 
Si3 Rb11 Si6 112.66(17) . . ? 
Si5 Rb11 Si6 116.17(16) . . ? 
Si5 Rb11 Si6 48.82(14) 2_645 . ? 
O61 Rb12 O50 98.2(4) . 2_645 ? 
O61 Rb12 O56 52.1(4) . . ? 
O50 Rb12 O56 52.6(4) 2_645 . ? 
O61 Rb12 Si6 25.0(3) . . ? 
O50 Rb12 Si6 75.0(3) 2_645 . ? 
O56 Rb12 Si6 27.3(3) . . ? 
O61 Rb12 Si5 74.9(3) . 2_645 ? 
O50 Rb12 Si5 25.1(3) 2_645 2_645 ? 
O56 Rb12 Si5 27.6(3) . 2_645 ? 
Si6 Rb12 Si5 50.65(15) . 2_645 ? 
O61 Rb12 Rb9 144.5(3) . 1_545 ? 
O50 Rb12 Rb9 46.9(3) 2_645 1_545 ? 
O56 Rb12 Rb9 97.4(3) . 1_545 ? 
Si6 Rb12 Rb9 121.84(13) . 1_545 ? 
Si5 Rb12 Rb9 71.32(12) 2_645 1_545 ? 
O61 Rb12 Si14 107.0(4) . 2_645 ? 
O50 Rb12 Si14 83.4(4) 2_645 2_645 ? 
O56 Rb12 Si14 118.2(3) . 2_645 ? 
Si6 Rb12 Si14 112.8(2) . 2_645 ? 
Si5 Rb12 Si14 99.1(2) 2_645 2_645 ? 
Rb9 Rb12 Si14 68.70(17) 1_545 2_645 ? 
O61 Rb12 Si14 126.1(4) . 4_565 ? 
O50 Rb12 Si14 123.8(3) 2_645 4_565 ? 
O56 Rb12 Si14 129.9(3) . 4_565 ? 
Si6 Rb12 Si14 135.3(2) . 4_565 ? 
Si5 Rb12 Si14 133.8(2) 2_645 4_565 ? 
Rb9 Rb12 Si14 86.15(17) 1_545 4_565 ? 
Si14 Rb12 Si14 109.7(2) 2_645 4_565 ? 
O61 Rb12 Si12 142.0(4) . 4_565 ? 
O50 Rb12 Si12 87.1(3) 2_645 4_565 ? 
O56 Rb12 Si12 107.8(3) . 4_565 ? 
Si6 Rb12 Si12 129.9(2) . 4_565 ? 
Si5 Rb12 Si12 99.53(18) 2_645 4_565 ? 
Rb9 Rb12 Si12 56.35(13) 1_545 4_565 ? 
Si14 Rb12 Si12 110.9(2) 2_645 4_565 ? 
Si14 Rb12 Si12 36.82(19) 4_565 4_565 ? 
O61 Rb12 Si13 107.4(3) . . ? 
O50 Rb12 Si13 104.8(3) 2_645 . ? 
O56 Rb12 Si13 93.8(3) . . ? 
Si6 Rb12 Si13 104.17(17) . . ? 
Si5 Rb12 Si13 102.61(17) 2_645 . ? 
Rb9 Rb12 Si13 90.44(13) 1_545 . ? 
Si14 Rb12 Si13 143.0(2) 2_645 . ? 
Si14 Rb12 Si13 36.05(19) 4_565 . ? 
Si12 Rb12 Si13 36.10(17) 4_565 . ? 
O61 Rb12 Rb5 46.5(3) . 2_645 ? 
O50 Rb12 Rb5 92.1(3) 2_645 2_645 ? 
O56 Rb12 Rb5 78.2(3) . 2_645 ? 
Si6 Rb12 Rb5 57.74(12) . 2_645 ? 
Si5 Rb12 Rb5 82.98(12) 2_645 2_645 ? 
Rb9 Rb12 Rb5 117.54(8) 1_545 2_645 ? 
Si14 Rb12 Rb5 60.49(17) 2_645 2_645 ? 
Si14 Rb12 Rb5 142.70(17) 4_565 2_645 ? 
Si12 Rb12 Rb5 171.42(16) 4_565 2_645 ? 
Si13 Rb12 Rb5 151.50(13) . 2_645 ? 
O61 Rb12 Rb7 93.5(3) . 4_565 ? 
O50 Rb12 Rb7 55.8(3) 2_645 4_565 ? 
O56 Rb12 Rb7 49.2(3) . 4_565 ? 
Si6 Rb12 Rb7 72.87(13) . 4_565 ? 
Si5 Rb12 Rb7 49.47(12) 2_645 4_565 ? 
Rb9 Rb12 Rb7 72.58(8) 1_545 4_565 ? 
Si14 Rb12 Rb7 136.75(17) 2_645 4_565 ? 
Si14 Rb12 Rb7 85.79(17) 4_565 4_565 ? 
Si12 Rb12 Rb7 58.71(16) 4_565 4_565 ? 
Si13 Rb12 Rb7 53.24(13) . 4_565 ? 
Rb5 Rb12 Rb7 127.19(9) 2_645 4_565 ? 
O11 Rb13 O20 83.5(5) 2_645 2_645 ? 
O11 Rb13 O60 131.3(5) 2_645 . ? 
O20 Rb13 O60 106.6(5) 2_645 . ? 
O11 Rb13 O23 130.1(5) 2_645 2_655 ? 
O20 Rb13 O23 53.0(4) 2_645 2_655 ? 
O60 Rb13 O23 88.5(4) . 2_655 ? 
O11 Rb13 O40 91.4(5) 2_645 2_655 ? 
O20 Rb13 O40 127.9(5) 2_645 2_655 ? 
O60 Rb13 O40 114.9(4) . 2_655 ? 
O23 Rb13 O40 97.2(4) 2_655 2_655 ? 
O11 Rb13 O46 85.9(4) 2_645 2_645 ? 
O20 Rb13 O46 88.3(4) 2_645 2_645 ? 
O60 Rb13 O46 48.2(4) . 2_645 ? 
O23 Rb13 O46 112.5(4) 2_655 2_645 ? 
O40 Rb13 O46 143.2(4) 2_655 2_645 ? 
O11 Rb13 O34 126.4(5) 2_645 2_655 ? 
O20 Rb13 O34 95.9(4) 2_645 2_655 ? 
O60 Rb13 O34 100.4(4) . 2_655 ? 
O23 Rb13 O34 50.2(4) 2_655 2_655 ? 
O40 Rb13 O34 47.9(5) 2_655 2_655 ? 
O46 Rb13 O34 147.7(4) 2_645 2_655 ? 
O11 Rb13 Si6 104.3(4) 2_645 . ? 
O20 Rb13 Si6 112.9(4) 2_645 . ? 
O60 Rb13 Si6 27.4(3) . . ? 
O23 Rb13 Si6 113.8(3) 2_655 . ? 
O40 Rb13 Si6 118.5(3) 2_655 . ? 
O46 Rb13 Si6 29.6(3) 2_645 . ? 
O34 Rb13 Si6 124.2(3) 2_655 . ? 
O11 Rb13 O61 90.2(5) 2_645 . ? 
O20 Rb13 O61 134.7(4) 2_645 . ? 
O60 Rb13 O61 48.5(4) . . ? 
O23 Rb13 O61 136.6(4) 2_655 . ? 
O40 Rb13 O61 97.0(4) 2_655 . ? 
O46 Rb13 O61 46.4(4) 2_645 . ? 
O34 Rb13 O61 122.7(4) 2_655 . ? 
Si6 Rb13 O61 26.7(3) . . ? 
O11 Rb13 Si4 118.1(4) 2_645 2_655 ? 
O20 Rb13 Si4 122.1(4) 2_645 2_655 ? 
O60 Rb13 Si4 96.9(3) . 2_655 ? 
O23 Rb13 Si4 76.3(3) 2_655 2_655 ? 
O40 Rb13 Si4 27.1(3) 2_655 2_655 ? 
O46 Rb13 Si4 141.4(3) 2_645 2_655 ? 
O34 Rb13 Si4 26.9(3) 2_655 2_655 ? 
Si6 Rb13 Si4 111.86(16) . 2_655 ? 
O61 Rb13 Si4 100.4(3) . 2_655 ? 
O11 Rb13 O45 133.0(5) 2_645 2_655 ? 
O20 Rb13 O45 135.4(4) 2_645 2_655 ? 
O60 Rb13 O45 70.9(4) . 2_655 ? 
O23 Rb13 O45 82.5(4) 2_655 2_655 ? 
O40 Rb13 O45 46.3(4) 2_655 2_655 ? 
O46 Rb13 O45 114.8(3) 2_645 2_655 ? 
O34 Rb13 O45 44.4(4) 2_655 2_655 ? 
Si6 Rb13 O45 85.4(3) . 2_655 ? 
O61 Rb13 O45 78.3(4) . 2_655 ? 
Si4 Rb13 O45 26.8(3) 2_655 2_655 ? 
O11 Rb13 Rb6 119.6(4) 2_645 2_645 ? 
O20 Rb13 Rb6 56.8(4) 2_645 2_645 ? 
O60 Rb13 Rb6 49.8(3) . 2_645 ? 
O23 Rb13 Rb6 59.2(3) 2_655 2_645 ? 
O40 Rb13 Rb6 148.4(3) 2_655 2_645 ? 
O46 Rb13 Rb6 53.3(3) 2_645 2_645 ? 
O34 Rb13 Rb6 103.2(3) 2_655 2_645 ? 
Si6 Rb13 Rb6 62.63(14) . 2_645 ? 
O61 Rb13 Rb6 89.3(3) . 2_645 ? 
Si4 Rb13 Rb6 121.24(15) 2_655 2_645 ? 
O45 Rb13 Rb6 105.8(3) 2_655 2_645 ? 
O10 Rb14 Si11 108.5(4) 2_645 2_655 ? 
O10 Rb14 Si12 107.0(3) 2_645 2_645 ? 
Si11 Rb14 Si12 132.9(2) 2_655 2_645 ? 
O10 Rb14 Rb2 48.6(4) 2_645 1_655 ? 
Si11 Rb14 Rb2 147.77(19) 2_655 1_655 ? 
Si12 Rb14 Rb2 79.28(16) 2_645 1_655 ? 
O10 Rb14 Si13 143.1(4) 2_645 3_665 ? 
Si11 Rb14 Si13 35.57(19) 2_655 3_665 ? 
Si12 Rb14 Si13 101.12(19) 2_645 3_665 ? 
Rb2 Rb14 Si13 164.08(17) 1_655 3_665 ? 
O10 Rb14 Rb3 48.6(3) 2_645 2_655 ? 
Si11 Rb14 Rb3 61.85(19) 2_655 2_655 ? 
Si12 Rb14 Rb3 132.3(2) 2_645 2_655 ? 
Rb2 Rb14 Rb3 96.64(9) 1_655 2_655 ? 
Si13 Rb14 Rb3 94.69(14) 3_665 2_655 ? 
O10 Rb14 Rb5 55.2(3) 2_645 2_645 ? 
Si11 Rb14 Rb5 122.0(2) 2_655 2_645 ? 
Si12 Rb14 Rb5 60.04(17) 2_645 2_645 ? 
Rb2 Rb14 Rb5 67.72(8) 1_655 2_645 ? 
Si13 Rb14 Rb5 126.46(16) 3_665 2_645 ? 
Rb3 Rb14 Rb5 74.36(9) 2_655 2_645 ? 
O10 Rb14 Rb9 136.6(4) 2_645 3_665 ? 
Si11 Rb14 Rb9 79.78(18) 2_655 3_665 ? 
Si12 Rb14 Rb9 53.13(15) 2_645 3_665 ? 
Rb2 Rb14 Rb9 132.29(10) 1_655 3_665 ? 
Si13 Rb14 Rb9 51.46(12) 3_665 3_665 ? 
Rb3 Rb14 Rb9 112.05(10) 2_655 3_665 ? 
Rb5 Rb14 Rb9 83.84(9) 2_645 3_665 ? 
O10 Rb14 Rb4 40.4(3) 2_645 1_655 ? 
Si11 Rb14 Rb4 87.14(17) 2_655 1_655 ? 
Si12 Rb14 Rb4 139.32(17) 2_645 1_655 ? 
Rb2 Rb14 Rb4 60.71(8) 1_655 1_655 ? 
Si13 Rb14 Rb4 119.33(13) 3_665 1_655 ? 
Rb3 Rb14 Rb4 52.93(6) 2_655 1_655 ? 
Rb5 Rb14 Rb4 95.58(8) 2_645 1_655 ? 
Rb9 Rb14 Rb4 164.04(10) 3_665 1_655 ? 
O10 Rb14 Rb4 154.4(4) 2_645 3_665 ? 
Si11 Rb14 Rb4 73.5(2) 2_655 3_665 ? 
Si12 Rb14 Rb4 87.14(16) 2_645 3_665 ? 
Rb2 Rb14 Rb4 116.80(11) 1_655 3_665 ? 
Si13 Rb14 Rb4 47.68(13) 3_665 3_665 ? 
Rb3 Rb14 Rb4 133.65(9) 2_655 3_665 ? 
Rb5 Rb14 Rb4 146.23(9) 2_645 3_665 ? 
Rb9 Rb14 Rb4 68.88(7) 3_665 3_665 ? 
Rb4 Rb14 Rb4 116.14(10) 1_655 3_665 ? 
O10 Rb14 Rb2 110.0(4) 2_645 3_655 ? 
Si11 Rb14 Rb2 132.8(2) 2_655 3_655 ? 
Si12 Rb14 Rb2 56.09(18) 2_645 3_655 ? 
Rb2 Rb14 Rb2 61.41(8) 1_655 3_655 ? 
Si13 Rb14 Rb2 105.37(14) 3_665 3_655 ? 
Rb3 Rb14 Rb2 156.46(10) 2_655 3_655 ? 
Rb5 Rb14 Rb2 102.22(9) 2_645 3_655 ? 
Rb9 Rb14 Rb2 90.35(8) 3_665 3_655 ? 
Rb4 Rb14 Rb2 105.31(10) 1_655 3_655 ? 
Rb4 Rb14 Rb2 60.04(7) 3_665 3_655 ? 
O10 Rb14 Rb14 99.3(3) 2_645 3_765 ? 
Si11 Rb14 Rb14 71.3(2) 2_655 3_765 ? 
Si12 Rb14 Rb14 130.9(2) 2_645 3_765 ? 
Rb2 Rb14 Rb14 88.88(12) 1_655 3_765 ? 
Si13 Rb14 Rb14 78.82(15) 3_665 3_765 ? 
Rb3 Rb14 Rb14 96.06(10) 2_655 3_765 ? 
Rb5 Rb14 Rb14 152.92(12) 2_645 3_765 ? 
Rb9 Rb14 Rb14 123.00(11) 3_665 3_765 ? 
Rb4 Rb14 Rb14 59.79(8) 1_655 3_765 ? 
Rb4 Rb14 Rb14 56.35(8) 3_665 3_765 ? 
Rb2 Rb14 Rb14 76.35(11) 3_655 3_765 ? 
O11 Si1 O10 116.2(10) 2_545 2_545 ? 
O11 Si1 O13 108.7(10) 2_545 . ? 
O10 Si1 O13 109.5(9) 2_545 . ? 
O11 Si1 O12 110.3(9) 2_545 . ? 
O10 Si1 O12 108.7(9) 2_545 . ? 
O13 Si1 O12 102.5(7) . . ? 
O11 Si1 Rb3 64.5(6) 2_545 2 ? 
O10 Si1 Rb3 68.3(6) 2_545 2 ? 
O13 Si1 Rb3 87.6(5) . 2 ? 
O12 Si1 Rb3 169.8(6) . 2 ? 
O11 Si1 Rb5 67.3(7) 2_545 2_545 ? 
O10 Si1 Rb5 79.8(6) 2_545 2_545 ? 
O13 Si1 Rb5 170.6(6) . 2_545 ? 
O12 Si1 Rb5 72.0(5) . 2_545 ? 
Rb3 Si1 Rb5 97.80(17) 2 2_545 ? 
O11 Si1 Rb4 129.7(7) 2_545 . ? 
O10 Si1 Rb4 53.6(6) 2_545 . ? 
O13 Si1 Rb4 55.9(6) . . ? 
O12 Si1 Rb4 119.6(6) . . ? 
Rb3 Si1 Rb4 67.14(14) 2 . ? 
Rb5 Si1 Rb4 133.4(2) 2_545 . ? 
O11 Si1 Rb2 146.8(8) 2_545 . ? 
O10 Si1 Rb2 50.4(6) 2_545 . ? 
O13 Si1 Rb2 104.5(6) . . ? 
O12 Si1 Rb2 60.8(6) . . ? 
Rb3 Si1 Rb2 118.2(2) 2 . ? 
Rb5 Si1 Rb2 79.81(16) 2_545 . ? 
Rb4 Si1 Rb2 71.17(15) . . ? 
O11 Si1 Rb1 56.4(7) 2_545 2_545 ? 
O10 Si1 Rb1 151.8(6) 2_545 2_545 ? 
O13 Si1 Rb1 98.3(6) . 2_545 ? 
O12 Si1 Rb1 58.5(6) . 2_545 ? 
Rb3 Si1 Rb1 119.3(2) 2 2_545 ? 
Rb5 Si1 Rb1 72.34(15) 2_545 2_545 ? 
Rb4 Si1 Rb1 154.1(2) . 2_545 ? 
Rb2 Si1 Rb1 118.30(18) . 2_545 ? 
O11 Si1 Rb1 53.6(7) 2_545 . ? 
O10 Si1 Rb1 133.8(6) 2_545 . ? 
O13 Si1 Rb1 55.1(6) . . ? 
O12 Si1 Rb1 117.0(6) . . ? 
Rb3 Si1 Rb1 67.80(13) 2 . ? 
Rb5 Si1 Rb1 119.9(2) 2_545 . ? 
Rb4 Si1 Rb1 95.80(16) . . ? 
Rb2 Si1 Rb1 159.5(2) . . ? 
Rb1 Si1 Rb1 67.32(13) 2_545 . ? 
O20 Si2 O21 115.8(10) 4_576 4_576 ? 
O20 Si2 O12 109.3(10) 4_576 4_566 ? 
O21 Si2 O12 108.2(9) 4_576 4_566 ? 
O20 Si2 O23 109.2(9) 4_576 4_566 ? 
O21 Si2 O23 109.2(9) 4_576 4_566 ? 
O12 Si2 O23 104.5(8) 4_566 4_566 ? 
O20 Si2 Rb3 66.1(6) 4_576 3_566 ? 
O21 Si2 Rb3 73.6(6) 4_576 3_566 ? 
O12 Si2 Rb3 77.7(6) 4_566 3_566 ? 
O23 Si2 Rb3 175.3(6) 4_566 3_566 ? 
O20 Si2 Rb6 69.8(7) 4_576 4_576 ? 
O21 Si2 Rb6 73.3(6) 4_576 4_576 ? 
O12 Si2 Rb6 178.5(7) 4_566 4_576 ? 
O23 Si2 Rb6 74.7(6) 4_566 4_576 ? 
Rb3 Si2 Rb6 102.92(19) 3_566 4_576 ? 
O20 Si2 Rb7 139.0(7) 4_576 . ? 
O21 Si2 Rb7 51.2(6) 4_576 . ? 
O12 Si2 Rb7 111.6(6) 4_566 . ? 
O23 Si2 Rb7 58.7(6) 4_566 . ? 
Rb3 Si2 Rb7 124.6(2) 3_566 . ? 
Rb6 Si2 Rb7 69.22(15) 4_576 . ? 
O20 Si2 Rb13 52.1(6) 4_576 3_666 ? 
O21 Si2 Rb13 135.3(7) 4_576 3_666 ? 
O12 Si2 Rb13 116.4(6) 4_566 3_666 ? 
O23 Si2 Rb13 57.3(6) 4_566 3_666 ? 
Rb3 Si2 Rb13 118.0(2) 3_566 3_666 ? 
Rb6 Si2 Rb13 62.02(13) 4_576 3_666 ? 
Rb7 Si2 Rb13 106.12(18) . 3_666 ? 
O20 Si2 Rb2 145.6(7) 4_576 4_566 ? 
O21 Si2 Rb2 50.2(6) 4_576 4_566 ? 
O12 Si2 Rb2 60.7(6) 4_566 4_566 ? 
O23 Si2 Rb2 105.3(6) 4_566 4_566 ? 
Rb3 Si2 Rb2 79.48(17) 3_566 4_566 ? 
Rb6 Si2 Rb2 120.8(2) 4_576 4_566 ? 
Rb7 Si2 Rb2 62.64(14) . 4_566 ? 
Rb13 Si2 Rb2 162.0(2) 3_666 4_566 ? 
O20 Si2 Rb1 52.8(7) 4_576 3_566 ? 
O21 Si2 Rb1 150.9(6) 4_576 3_566 ? 
O12 Si2 Rb1 61.6(6) 4_566 3_566 ? 
O23 Si2 Rb1 99.9(6) 4_566 3_566 ? 
Rb3 Si2 Rb1 77.41(17) 3_566 3_566 ? 
Rb6 Si2 Rb1 117.1(2) 4_576 3_566 ? 
Rb7 Si2 Rb1 156.6(2) . 3_566 ? 
Rb13 Si2 Rb1 63.42(15) 3_666 3_566 ? 
Rb2 Si2 Rb1 120.95(19) 4_566 3_566 ? 
O20 Si2 Rb4 91.0(7) 4_576 4_576 ? 
O21 Si2 Rb4 24.9(6) 4_576 4_576 ? 
O12 Si2 Rb4 121.1(6) 4_566 4_576 ? 
O23 Si2 Rb4 120.2(6) 4_566 4_576 ? 
Rb3 Si2 Rb4 60.88(13) 3_566 4_576 ? 
Rb6 Si2 Rb4 60.32(13) 4_576 4_576 ? 
Rb7 Si2 Rb4 69.24(14) . 4_576 ? 
Rb13 Si2 Rb4 119.31(18) 3_666 4_576 ? 
Rb2 Si2 Rb4 71.51(15) 4_566 4_576 ? 
Rb1 Si2 Rb4 134.08(19) 3_566 4_576 ? 
O30 Si3 O23 111.7(10) . . ? 
O30 Si3 O13 115.6(10) . . ? 
O23 Si3 O13 106.6(8) . . ? 
O30 Si3 O34 110.8(10) . . ? 
O23 Si3 O34 107.0(9) . . ? 
O13 Si3 O34 104.6(9) . . ? 
O30 Si3 Rb6 60.6(8) . . ? 
O23 Si3 Rb6 168.5(6) . . ? 
O13 Si3 Rb6 84.8(5) . . ? 
O34 Si3 Rb6 70.4(6) . . ? 
O30 Si3 Rb11 60.6(7) . . ? 
O23 Si3 Rb11 74.0(6) . . ? 
O13 Si3 Rb11 175.7(7) . . ? 
O34 Si3 Rb11 79.1(6) . . ? 
Rb6 Si3 Rb11 94.54(16) . . ? 
O30 Si3 Rb4 63.0(7) . . ? 
O23 Si3 Rb4 120.6(7) . . ? 
O13 Si3 Rb4 53.1(6) . . ? 
O34 Si3 Rb4 131.1(6) . . ? 
Rb6 Si3 Rb4 65.13(13) . . ? 
Rb11 Si3 Rb4 122.8(2) . . ? 
O30 Si3 Rb7 58.3(8) . 4_565 ? 
O23 Si3 Rb7 57.2(6) . 4_565 ? 
O13 Si3 Rb7 111.8(6) . 4_565 ? 
O34 Si3 Rb7 143.1(6) . 4_565 ? 
Rb6 Si3 Rb7 117.9(2) . 4_565 ? 
Rb11 Si3 Rb7 64.76(13) . 4_565 ? 
Rb4 Si3 Rb7 78.57(17) . 4_565 ? 
O30 Si3 Rb13 130.2(7) . 2_645 ? 
O23 Si3 Rb13 49.6(6) . 2_645 ? 
O13 Si3 Rb13 114.1(6) . 2_645 ? 
O34 Si3 Rb13 57.5(6) . 2_645 ? 
Rb6 Si3 Rb13 127.2(2) . 2_645 ? 
Rb11 Si3 Rb13 69.64(13) . 2_645 ? 
Rb4 Si3 Rb13 163.9(2) . 2_645 ? 
Rb7 Si3 Rb13 100.55(16) 4_565 2_645 ? 
O30 Si3 Rb1 129.8(8) . . ? 
O23 Si3 Rb1 118.3(7) . . ? 
O13 Si3 Rb1 53.4(6) . . ? 
O34 Si3 Rb1 51.2(6) . . ? 
Rb6 Si3 Rb1 69.29(14) . . ? 
Rb11 Si3 Rb1 130.2(2) . . ? 
Rb4 Si3 Rb1 93.45(16) . . ? 
Rb7 Si3 Rb1 164.3(2) 4_565 . ? 
Rb13 Si3 Rb1 83.36(16) 2_645 . ? 
O40 Si4 O34 112.0(10) . . ? 
O40 Si4 O45 112.4(9) . . ? 
O34 Si4 O45 108.4(9) . . ? 
O40 Si4 O46 110.8(9) . . ? 
O34 Si4 O46 106.2(9) . . ? 
O45 Si4 O46 106.7(8) . . ? 
O40 Si4 Rb13 65.1(6) . 2_645 ? 
O34 Si4 Rb13 71.0(7) . 2_645 ? 
O45 Si4 Rb13 80.8(5) . 2_645 ? 
O46 Si4 Rb13 172.6(6) . 2_645 ? 
O40 Si4 Rb1 72.3(6) . . ? 
O34 Si4 Rb1 64.2(7) . . ? 
O45 Si4 Rb1 172.6(7) . . ? 
O46 Si4 Rb1 76.0(5) . . ? 
Rb13 Si4 Rb1 96.64(17) 2_645 . ? 
O40 Si4 Rb8 54.2(6) . . ? 
O34 Si4 Rb8 133.9(7) . . ? 
O45 Si4 Rb8 58.6(6) . . ? 
O46 Si4 Rb8 119.9(6) . . ? 
Rb13 Si4 Rb8 63.40(13) 2_645 . ? 
Rb1 Si4 Rb8 126.5(2) . . ? 
O40 Si4 Rb5 52.7(6) . . ? 
O34 Si4 Rb5 136.6(7) . . ? 
O45 Si4 Rb5 114.9(6) . . ? 
O46 Si4 Rb5 59.6(6) . . ? 
Rb13 Si4 Rb5 117.4(2) 2_645 . ? 
Rb1 Si4 Rb5 72.46(14) . . ? 
Rb8 Si4 Rb5 74.90(16) . . ? 
O40 Si4 Rb6 140.9(6) . . ? 
O34 Si4 Rb6 57.2(7) . . ? 
O45 Si4 Rb6 106.4(6) . . ? 
O46 Si4 Rb6 51.4(6) . . ? 
Rb13 Si4 Rb6 127.5(2) 2_645 . ? 
Rb1 Si4 Rb6 69.58(13) . . ? 
Rb8 Si4 Rb6 162.0(2) . . ? 
Rb5 Si4 Rb6 106.36(16) . . ? 
O40 Si4 Rb11 131.2(6) . . ? 
O34 Si4 Rb11 64.9(7) . . ? 
O45 Si4 Rb11 43.5(6) . . ? 
O46 Si4 Rb11 116.7(6) . . ? 
Rb13 Si4 Rb11 68.80(13) 2_645 . ? 
Rb1 Si4 Rb11 129.0(2) . . ? 
Rb8 Si4 Rb11 91.41(15) . . ? 
Rb5 Si4 Rb11 158.11(19) . . ? 
Rb6 Si4 Rb11 81.47(15) . . ? 
O51 Si5 O50 113.2(9) . . ? 
O51 Si5 O45 109.4(9) . . ? 
O50 Si5 O45 110.0(9) . . ? 
O51 Si5 O56 111.6(9) . 2_655 ? 
O50 Si5 O56 109.1(8) . 2_655 ? 
O45 Si5 O56 103.0(7) . 2_655 ? 
O51 Si5 Rb7 65.1(6) . 3_666 ? 
O50 Si5 Rb7 83.0(6) . 3_666 ? 
O45 Si5 Rb7 166.9(6) . 3_666 ? 
O56 Si5 Rb7 69.9(5) 2_655 3_666 ? 
O51 Si5 Rb10 62.6(6) . 2_645 ? 
O50 Si5 Rb10 64.3(6) . 2_645 ? 
O45 Si5 Rb10 92.1(5) . 2_645 ? 
O56 Si5 Rb10 164.9(6) 2_655 2_645 ? 
Rb7 Si5 Rb10 95.37(18) 3_666 2_645 ? 
O51 Si5 Rb8 130.6(6) . . ? 
O50 Si5 Rb8 52.0(6) . . ? 
O45 Si5 Rb8 58.1(6) . . ? 
O56 Si5 Rb8 117.8(6) 2_655 . ? 
Rb7 Si5 Rb8 134.8(2) 3_666 . ? 
Rb10 Si5 Rb8 70.03(15) 2_645 . ? 
O51 Si5 Rb12 136.8(6) . 2_655 ? 
O50 Si5 Rb12 53.0(6) . 2_655 ? 
O45 Si5 Rb12 113.7(6) . 2_655 ? 
O56 Si5 Rb12 56.5(5) 2_655 2_655 ? 
Rb7 Si5 Rb12 72.25(14) 3_666 2_655 ? 
Rb10 Si5 Rb12 116.9(2) 2_645 2_655 ? 
Rb8 Si5 Rb12 77.09(16) . 2_655 ? 
O51 Si5 Rb11 52.3(6) . . ? 
O50 Si5 Rb11 129.7(6) . . ? 
O45 Si5 Rb11 57.2(6) . . ? 
O56 Si5 Rb11 121.0(6) 2_655 . ? 
Rb7 Si5 Rb11 116.2(2) 3_666 . ? 
Rb10 Si5 Rb11 67.74(13) 2_645 . ? 
Rb8 Si5 Rb11 97.89(16) . . ? 
Rb12 Si5 Rb11 170.6(2) 2_655 . ? 
O51 Si5 Rb11 57.2(6) . 2_655 ? 
O50 Si5 Rb11 149.8(6) . 2_655 ? 
O45 Si5 Rb11 100.0(6) . 2_655 ? 
O56 Si5 Rb11 59.0(6) 2_655 2_655 ? 
Rb7 Si5 Rb11 66.92(15) 3_666 2_655 ? 
Rb10 Si5 Rb11 119.2(2) 2_645 2_655 ? 
Rb8 Si5 Rb11 157.6(2) . 2_655 ? 
Rb12 Si5 Rb11 111.67(17) 2_655 2_655 ? 
Rb11 Si5 Rb11 70.24(14) . 2_655 ? 
O60 Si6 O61 117.5(9) . . ? 
O60 Si6 O56 110.3(10) . . ? 
O61 Si6 O56 109.7(8) . . ? 
O60 Si6 O46 105.7(8) . 2_645 ? 
O61 Si6 O46 107.3(9) . 2_645 ? 
O56 Si6 O46 105.5(8) . 2_645 ? 
O60 Si6 Rb10 65.9(6) . . ? 
O61 Si6 Rb10 77.0(6) . . ? 
O56 Si6 Rb10 79.2(5) . . ? 
O46 Si6 Rb10 171.6(6) 2_645 . ? 
O60 Si6 Rb13 64.9(7) . . ? 
O61 Si6 Rb13 77.1(6) . . ? 
O56 Si6 Rb13 173.2(6) . . ? 
O46 Si6 Rb13 72.2(5) 2_645 . ? 
Rb10 Si6 Rb13 102.27(17) . . ? 
O60 Si6 Rb12 141.2(6) . . ? 
O61 Si6 Rb12 50.8(6) . . ? 
O56 Si6 Rb12 59.4(6) . . ? 
O46 Si6 Rb12 113.0(6) 2_645 . ? 
Rb10 Si6 Rb12 75.33(15) . . ? 
Rb13 Si6 Rb12 127.4(2) . . ? 
O60 Si6 Rb6 48.4(6) . 2_645 ? 
O61 Si6 Rb6 138.7(6) . 2_645 ? 
O56 Si6 Rb6 111.5(6) . 2_645 ? 
O46 Si6 Rb6 58.5(5) 2_645 2_645 ? 
Rb10 Si6 Rb6 113.5(2) . 2_645 ? 
Rb13 Si6 Rb6 61.79(13) . 2_645 ? 
Rb12 Si6 Rb6 167.0(2) . 2_645 ? 
O60 Si6 Rb5 138.5(7) . 2_645 ? 
O61 Si6 Rb5 49.5(6) . 2_645 ? 
O56 Si6 Rb5 111.1(6) . 2_645 ? 
O46 Si6 Rb5 59.1(6) 2_645 2_645 ? 
Rb10 Si6 Rb5 126.2(2) . 2_645 ? 
Rb13 Si6 Rb5 73.53(15) . 2_645 ? 
Rb12 Si6 Rb5 67.73(14) . 2_645 ? 
Rb6 Si6 Rb5 110.71(18) 2_645 2_645 ? 
O60 Si6 Rb11 55.2(7) . . ? 
O61 Si6 Rb11 149.4(7) . . ? 
O56 Si6 Rb11 57.7(6) . . ? 
O46 Si6 Rb11 103.1(6) 2_645 . ? 
Rb10 Si6 Rb11 73.26(15) . . ? 
Rb13 Si6 Rb11 116.1(2) . . ? 
Rb12 Si6 Rb11 113.23(18) . . ? 
Rb6 Si6 Rb11 62.95(13) 2_645 . ? 
Rb5 Si6 Rb11 157.64(19) 2_645 . ? 
O60 Si6 Rb8 88.5(7) . 2_655 ? 
O61 Si6 Rb8 29.2(6) . 2_655 ? 
O56 Si6 Rb8 127.5(6) . 2_655 ? 
O46 Si6 Rb8 116.0(6) 2_645 2_655 ? 
Rb10 Si6 Rb8 64.27(12) . 2_655 ? 
Rb13 Si6 Rb8 58.32(12) . 2_655 ? 
Rb12 Si6 Rb8 75.16(14) . 2_655 ? 
Rb6 Si6 Rb8 116.92(17) 2_645 2_655 ? 
Rb5 Si6 Rb8 69.33(13) 2_645 2_655 ? 
Rb11 Si6 Rb8 133.02(17) . 2_655 ? 
Si12 Si11 Si13 60.2(3) . 4_566 ? 
Si12 Si11 Si14 59.6(4) . . ? 
Si13 Si11 Si14 58.7(4) 4_566 . ? 
Si12 Si11 Rb14 147.3(4) . 2_645 ? 
Si13 Si11 Rb14 88.6(3) 4_566 2_645 ? 
Si14 Si11 Rb14 96.8(4) . 2_645 ? 
Si12 Si11 Rb2 102.1(4) . 2 ? 
Si13 Si11 Rb2 141.1(5) 4_566 2 ? 
Si14 Si11 Rb2 145.6(5) . 2 ? 
Rb14 Si11 Rb2 109.1(3) 2_645 2 ? 
Si12 Si11 Rb5 73.8(3) . . ? 
Si13 Si11 Rb5 124.8(4) 4_566 . ? 
Si14 Si11 Rb5 72.9(4) . . ? 
Rb14 Si11 Rb5 123.8(3) 2_645 . ? 
Rb2 Si11 Rb5 73.98(19) 2 . ? 
Si12 Si11 Rb2 71.8(4) . 4_566 ? 
Si13 Si11 Rb2 71.7(4) 4_566 4_566 ? 
Si14 Si11 Rb2 122.4(4) . 4_566 ? 
Rb14 Si11 Rb2 109.9(3) 2_645 4_566 ? 
Rb2 Si11 Rb2 69.8(2) 2 4_566 ? 
Rb5 Si11 Rb2 122.3(3) . 4_566 ? 
Si12 Si11 Rb3 132.9(5) . . ? 
Si13 Si11 Rb3 146.8(5) 4_566 . ? 
Si14 Si11 Rb3 99.0(4) . . ? 
Rb14 Si11 Rb3 68.62(19) 2_645 . ? 
Rb2 Si11 Rb3 71.39(17) 2 . ? 
Rb5 Si11 Rb3 59.41(17) . . ? 
Rb2 Si11 Rb3 137.9(3) 4_566 . ? 
Si11 Si12 Si13 60.3(4) . 4_566 ? 
Si11 Si12 Si14 61.7(4) . . ? 
Si13 Si12 Si14 59.4(4) 4_566 . ? 
Si11 Si12 Rb14 100.9(4) . 2_655 ? 
Si13 Si12 Rb14 145.6(4) 4_566 2_655 ? 
Si14 Si12 Rb14 140.5(4) . 2_655 ? 
Si11 Si12 Rb9 169.3(5) . 4_576 ? 
Si13 Si12 Rb9 128.9(4) 4_566 4_576 ? 
Si14 Si12 Rb9 116.5(4) . 4_576 ? 
Rb14 Si12 Rb9 73.77(17) 2_655 4_576 ? 
Si11 Si12 Rb12 125.0(4) . 4_566 ? 
Si13 Si12 Rb12 73.4(3) 4_566 4_566 ? 
Si14 Si12 Rb12 70.2(3) . 4_566 ? 
Rb14 Si12 Rb12 133.7(2) 2_655 4_566 ? 
Rb9 Si12 Rb12 60.03(16) 4_576 4_566 ? 
Si11 Si12 Rb7 113.8(4) . . ? 
Si13 Si12 Rb7 64.5(3) 4_566 . ? 
Si14 Si12 Rb7 114.8(4) . . ? 
Rb14 Si12 Rb7 104.6(2) 2_655 . ? 
Rb9 Si12 Rb7 76.72(18) 4_576 . ? 
Rb12 Si12 Rb7 64.25(15) 4_566 . ? 
Si11 Si12 Rb2 72.8(4) . 4_566 ? 
Si13 Si12 Rb2 72.2(3) 4_566 4_566 ? 
Si14 Si12 Rb2 124.9(4) . 4_566 ? 
Rb14 Si12 Rb2 74.7(2) 2_655 4_566 ? 
Rb9 Si12 Rb2 113.7(2) 4_576 4_566 ? 
Rb12 Si12 Rb2 120.6(2) 4_566 4_566 ? 
Rb7 Si12 Rb2 57.55(15) . 4_566 ? 
Si11 Si12 Rb5 70.9(3) . . ? 
Si13 Si12 Rb5 122.4(3) 4_566 . ? 
Si14 Si12 Rb5 72.0(3) . . ? 
Rb14 Si12 Rb5 68.71(17) 2_655 . ? 
Rb9 Si12 Rb5 98.4(2) 4_576 . ? 
Rb12 Si12 Rb5 118.1(3) 4_566 . ? 
Rb7 Si12 Rb5 172.8(2) . . ? 
Rb2 Si12 Rb5 121.2(2) 4_566 . ? 
Si14 Si13 Si12 60.5(4) 4_565 4_565 ? 
Si14 Si13 Si11 61.8(4) 4_565 4_565 ? 
Si12 Si13 Si11 59.5(4) 4_565 4_565 ? 
Si14 Si13 Rb4 151.8(4) 4_565 . ? 
Si12 Si13 Rb4 140.2(4) 4_565 . ? 
Si11 Si13 Rb4 108.2(4) 4_565 . ? 
Si14 Si13 Rb7 127.1(4) 4_565 4_565 ? 
Si12 Si13 Rb7 78.5(3) 4_565 4_565 ? 
Si11 Si13 Rb7 124.3(4) 4_565 4_565 ? 
Rb4 Si13 Rb7 80.78(19) . 4_565 ? 
Si14 Si13 Rb9 72.4(3) 4_565 . ? 
Si12 Si13 Rb9 131.3(4) 4_565 . ? 
Si11 Si13 Rb9 108.9(4) 4_565 . ? 
Rb4 Si13 Rb9 88.16(18) . . ? 
Rb7 Si13 Rb9 126.5(2) 4_565 . ? 
Si14 Si13 Rb10 120.1(4) 4_565 . ? 
Si12 Si13 Rb10 129.8(3) 4_565 . ? 
Si11 Si13 Rb10 170.7(4) 4_565 . ? 
Rb4 Si13 Rb10 65.64(15) . . ? 
Rb7 Si13 Rb10 62.82(14) 4_565 . ? 
Rb9 Si13 Rb10 64.97(14) . . ? 
Si14 Si13 Rb12 69.1(3) 4_565 . ? 
Si12 Si13 Rb12 70.5(3) 4_565 . ? 
Si11 Si13 Rb12 121.9(4) 4_565 . ? 
Rb4 Si13 Rb12 129.5(2) . . ? 
Rb7 Si13 Rb12 66.49(14) 4_565 . ? 
Rb9 Si13 Rb12 82.41(18) . . ? 
Rb10 Si13 Rb12 65.45(14) . . ? 
Si14 Si13 Rb2 125.8(4) 4_565 . ? 
Si12 Si13 Rb2 72.1(3) 4_565 . ? 
Si11 Si13 Rb2 72.6(4) 4_565 . ? 
Rb4 Si13 Rb2 68.11(16) . . ? 
Rb7 Si13 Rb2 59.98(14) 4_565 . ? 
Rb9 Si13 Rb2 154.8(3) . . ? 
Rb10 Si13 Rb2 109.7(2) . . ? 
Rb12 Si13 Rb2 118.9(2) . . ? 
Si14 Si13 Rb14 81.2(3) 4_565 3_665 ? 
Si12 Si13 Rb14 114.5(3) 4_565 3_665 ? 
Si11 Si13 Rb14 55.8(3) 4_565 3_665 ? 
Rb4 Si13 Rb14 72.33(16) . 3_665 ? 
Rb7 Si13 Rb14 150.1(3) 4_565 3_665 ? 
Rb9 Si13 Rb14 66.44(14) . 3_665 ? 
Rb10 Si13 Rb14 114.95(19) . 3_665 ? 
Rb12 Si13 Rb14 142.3(2) . 3_665 ? 
Rb2 Si13 Rb14 97.01(19) . 3_665 ? 
Si13 Si14 Si12 60.2(4) 4_566 . ? 
Si13 Si14 Si11 59.5(4) 4_566 . ? 
Si12 Si14 Si11 58.6(4) . . ? 
Si13 Si14 Rb8 141.3(5) 4_566 . ? 
Si12 Si14 Rb8 144.6(4) . . ? 
Si11 Si14 Rb8 103.7(4) . . ? 
Si13 Si14 Rb9 69.9(3) 4_566 4_566 ? 
Si12 Si14 Rb9 128.6(4) . 4_566 ? 
Si11 Si14 Rb9 106.0(4) . 4_566 ? 
Rb8 Si14 Rb9 84.1(2) . 4_566 ? 
Si13 Si14 Rb12 140.8(4) 4_566 2_655 ? 
Si12 Si14 Rb12 92.4(4) . 2_655 ? 
Si11 Si14 Rb12 131.7(4) . 2_655 ? 
Rb8 Si14 Rb12 77.3(2) . 2_655 ? 
Rb9 Si14 Rb12 121.9(3) 4_566 2_655 ? 
Si13 Si14 Rb12 74.9(3) 4_566 4_566 ? 
Si12 Si14 Rb12 73.0(3) . 4_566 ? 
Si11 Si14 Rb12 124.9(4) . 4_566 ? 
Rb8 Si14 Rb12 131.4(3) . 4_566 ? 
Rb9 Si14 Rb12 83.4(2) 4_566 4_566 ? 
Rb12 Si14 Rb12 70.3(2) 2_655 4_566 ? 
Si13 Si14 Rb5 123.6(4) 4_566 . ? 
Si12 Si14 Rb5 72.6(3) . . ? 
Si11 Si14 Rb5 70.6(3) . . ? 
Rb8 Si14 Rb5 72.54(19) . . ? 
Rb9 Si14 Rb5 154.3(3) 4_566 . ? 
Rb12 Si14 Rb5 63.69(17) 2_655 . ? 
Rb12 Si14 Rb5 119.9(3) 4_566 . ? 
Si1 O10 Rb14 155.8(9) 2 2_655 ? 
Si1 O10 Rb2 104.2(7) 2 2 ? 
Rb14 O10 Rb2 85.9(5) 2_655 2 ? 
Si1 O10 Rb4 99.9(7) 2 2 ? 
Rb14 O10 Rb4 101.6(5) 2_655 2 ? 
Rb2 O10 Rb4 92.5(5) 2 2 ? 
Si1 O10 Rb3 83.2(7) 2 1_565 ? 
Rb14 O10 Rb3 90.3(4) 2_655 1_565 ? 
Rb2 O10 Rb3 169.3(6) 2 1_565 ? 
Rb4 O10 Rb3 78.4(4) 2 1_565 ? 
Si1 O10 Rb5 73.4(6) 2 . ? 
Rb14 O10 Rb5 84.9(4) 2_655 . ? 
Rb2 O10 Rb5 89.5(4) 2 . ? 
Rb4 O10 Rb5 173.3(6) 2 . ? 
Rb3 O10 Rb5 100.1(4) 1_565 . ? 
Si1 O11 Rb13 175.1(12) 2 2_655 ? 
Si1 O11 Rb3 86.9(7) 2 1_565 ? 
Rb13 O11 Rb3 90.2(5) 2_655 1_565 ? 
Si1 O11 Rb5 84.8(8) 2 . ? 
Rb13 O11 Rb5 92.6(5) 2_655 . ? 
Rb3 O11 Rb5 110.9(6) 1_565 . ? 
Si1 O11 Rb1 98.9(8) 2 . ? 
Rb13 O11 Rb1 84.9(5) 2_655 . ? 
Rb3 O11 Rb1 164.4(7) 1_565 . ? 
Rb5 O11 Rb1 84.2(4) . . ? 
Si1 O11 Rb1 102.7(9) 2 2 ? 
Rb13 O11 Rb1 80.7(5) 2_655 2 ? 
Rb3 O11 Rb1 81.3(4) 1_565 2 ? 
Rb5 O11 Rb1 166.3(6) . 2 ? 
Rb1 O11 Rb1 83.3(5) . 2 ? 
Si2 O12 Si1 136.6(10) 4_565 . ? 
Si2 O12 Rb2 91.9(7) 4_565 . ? 
Si1 O12 Rb2 91.4(7) . . ? 
Si2 O12 Rb1 91.5(7) 4_565 2_545 ? 
Si1 O12 Rb1 95.1(7) . 2_545 ? 
Rb2 O12 Rb1 166.4(5) . 2_545 ? 
Si2 O12 Rb5 144.4(8) 4_565 2_545 ? 
Si1 O12 Rb5 78.9(6) . 2_545 ? 
Rb2 O12 Rb5 88.5(4) . 2_545 ? 
Rb1 O12 Rb5 81.1(4) 2_545 2_545 ? 
Si2 O12 Rb3 73.0(5) 4_565 2_545 ? 
Si1 O12 Rb3 150.3(8) . 2_545 ? 
Rb2 O12 Rb3 85.5(4) . 2_545 ? 
Rb1 O12 Rb3 83.0(4) 2_545 2_545 ? 
Rb5 O12 Rb3 71.5(3) 2_545 2_545 ? 
Si3 O13 Si1 136.2(9) . . ? 
Si3 O13 Rb4 100.3(7) . . ? 
Si1 O13 Rb4 96.2(7) . . ? 
Si3 O13 Rb1 102.3(7) . . ? 
Si1 O13 Rb1 100.0(7) . . ? 
Rb4 O13 Rb1 126.0(4) . . ? 
Si2 O20 Rb1 163.5(11) 4_575 . ? 
Si2 O20 Rb13 102.7(7) 4_575 2_655 ? 
Rb1 O20 Rb13 86.6(5) . 2_655 ? 
Si2 O20 Rb3 85.0(7) 4_575 2 ? 
Rb1 O20 Rb3 87.0(4) . 2 ? 
Rb13 O20 Rb3 171.0(7) 2_655 2 ? 
Si2 O20 Rb1 102.4(8) 4_575 2 ? 
Rb1 O20 Rb1 92.4(5) . 2 ? 
Rb13 O20 Rb1 80.7(5) 2_655 2 ? 
Rb3 O20 Rb1 93.2(5) 2 2 ? 
Si2 O20 Rb6 82.1(7) 4_575 . ? 
Rb1 O20 Rb6 88.0(5) . . ? 
Rb13 O20 Rb6 72.2(4) 2_655 . ? 
Rb3 O20 Rb6 114.0(6) 2 . ? 
Rb1 O20 Rb6 152.9(6) 2 . ? 
Si2 O21 Rb4 140.8(9) 4_575 . ? 
Si2 O21 Rb2 104.3(7) 4_575 1_565 ? 
Rb4 O21 Rb2 108.0(6) . 1_565 ? 
Si2 O21 Rb7 102.9(7) 4_575 4_575 ? 
Rb4 O21 Rb7 103.2(5) . 4_575 ? 
Rb2 O21 Rb7 81.5(4) 1_565 4_575 ? 
Si2 O21 Rb3 77.6(6) 4_575 2 ? 
Rb4 O21 Rb3 79.2(4) . 2 ? 
Rb2 O21 Rb3 92.9(4) 1_565 2 ? 
Rb7 O21 Rb3 174.4(6) 4_575 2 ? 
Si2 O21 Rb6 78.4(7) 4_575 . ? 
Rb4 O21 Rb6 78.1(4) . . ? 
Rb2 O21 Rb6 161.1(5) 1_565 . ? 
Rb7 O21 Rb6 79.7(4) 4_575 . ? 
Rb3 O21 Rb6 105.9(5) 2 . ? 
Si3 O23 Si2 133.1(10) . 4_565 ? 
Si3 O23 Rb13 106.1(8) . 2_645 ? 
Si2 O23 Rb13 94.9(6) 4_565 2_645 ? 
Si3 O23 Rb7 96.1(7) . 4_565 ? 
Si2 O23 Rb7 93.3(7) 4_565 4_565 ? 
Rb13 O23 Rb7 140.1(5) 2_645 4_565 ? 
Si3 O23 Rb6 151.0(8) . 1_545 ? 
Si2 O23 Rb6 75.7(5) 4_565 1_545 ? 
Rb13 O23 Rb6 68.4(3) 2_645 1_545 ? 
Rb7 O23 Rb6 76.0(4) 4_565 1_545 ? 
Si3 O23 Rb11 79.3(6) . . ? 
Si2 O23 Rb11 146.5(8) 4_565 . ? 
Rb13 O23 Rb11 80.4(3) 2_645 . ? 
Rb7 O23 Rb11 71.6(3) 4_565 . ? 
Rb6 O23 Rb11 71.7(3) 1_545 . ? 
Si3 O30 Rb10 174.8(12) . . ? 
Si3 O30 Rb6 91.7(9) . . ? 
Rb10 O30 Rb6 88.2(5) . . ? 
Si3 O30 Rb7 96.1(9) . 4_565 ? 
Rb10 O30 Rb7 83.0(5) . 4_565 ? 
Rb6 O30 Rb7 165.9(7) . 4_565 ? 
Si3 O30 Rb11 93.4(8) . . ? 
Rb10 O30 Rb11 91.4(5) . . ? 
Rb6 O30 Rb11 114.7(7) . . ? 
Rb7 O30 Rb11 76.6(4) 4_565 . ? 
Si3 O30 Rb4 91.0(8) . . ? 
Rb10 O30 Rb4 83.9(5) . . ? 
Rb6 O30 Rb4 75.2(4) . . ? 
Rb7 O30 Rb4 92.9(6) 4_565 . ? 
Rb11 O30 Rb4 169.0(8) . . ? 
Si4 O34 Si3 166.2(12) . . ? 
Si4 O34 Rb1 89.4(8) . . ? 
Si3 O34 Rb1 104.1(7) . . ? 
Si4 O34 Rb6 99.1(8) . . ? 
Si3 O34 Rb6 80.2(7) . . ? 
Rb1 O34 Rb6 81.6(4) . . ? 
Si4 O34 Rb13 82.1(7) . 2_645 ? 
Si3 O34 Rb13 96.6(7) . 2_645 ? 
Rb1 O34 Rb13 107.3(5) . 2_645 ? 
Rb6 O34 Rb13 171.0(6) . 2_645 ? 
Si4 O40 Rb3 167.9(9) . . ? 
Si4 O40 Rb8 100.1(8) . . ? 
Rb3 O40 Rb8 88.9(5) . . ? 
Si4 O40 Rb5 102.8(7) . . ? 
Rb3 O40 Rb5 84.1(5) . . ? 
Rb8 O40 Rb5 95.8(5) . . ? 
Si4 O40 Rb13 87.8(7) . 2_645 ? 
Rb3 O40 Rb13 86.7(4) . 2_645 ? 
Rb8 O40 Rb13 74.8(4) . 2_645 ? 
Rb5 O40 Rb13 167.0(6) . 2_645 ? 
Si4 O40 Rb1 81.6(6) . . ? 
Rb3 O40 Rb1 89.5(4) . . ? 
Rb8 O40 Rb1 178.2(7) . . ? 
Rb5 O40 Rb1 83.3(4) . . ? 
Rb13 O40 Rb1 105.9(5) 2_645 . ? 
Si4 O45 Si5 134.6(10) . . ? 
Si4 O45 Rb8 94.3(7) . . ? 
Si5 O45 Rb8 93.5(7) . . ? 
Si4 O45 Rb11 115.3(8) . . ? 
Si5 O45 Rb11 95.3(7) . . ? 
Rb8 O45 Rb11 125.8(5) . . ? 
Si4 O45 Rb13 72.4(5) . 2_645 ? 
Si5 O45 Rb13 149.7(7) . 2_645 ? 
Rb8 O45 Rb13 67.2(3) . 2_645 ? 
Rb11 O45 Rb13 79.6(3) . 2_645 ? 
Si4 O46 Si6 133.1(9) . 2_655 ? 
Si4 O46 Rb6 103.8(7) . . ? 
Si6 O46 Rb6 93.7(6) 2_655 . ? 
Si4 O46 Rb5 93.8(7) . . ? 
Si6 O46 Rb5 93.8(6) 2_655 . ? 
Rb6 O46 Rb5 147.5(5) . . ? 
Si4 O46 Rb13 148.7(7) . 2_655 ? 
Si6 O46 Rb13 78.2(6) 2_655 2_655 ? 
Rb6 O46 Rb13 68.7(3) . 2_655 ? 
Rb5 O46 Rb13 82.1(4) . 2_655 ? 
Si4 O46 Rb1 76.7(5) . . ? 
Si6 O46 Rb1 150.1(7) 2_655 . ? 
Rb6 O46 Rb1 78.9(3) . . ? 
Rb5 O46 Rb1 78.9(3) . . ? 
Rb13 O46 Rb1 72.1(3) 2_655 . ? 
Si5 O50 Rb9 164.7(9) . 2_645 ? 
Si5 O50 Rb8 102.2(7) . . ? 
Rb9 O50 Rb8 92.3(5) 2_645 . ? 
Si5 O50 Rb10 87.0(6) . 2_645 ? 
Rb9 O50 Rb10 89.2(4) 2_645 2_645 ? 
Rb8 O50 Rb10 84.7(4) . 2_645 ? 
Si5 O50 Rb12 101.9(7) . 2_655 ? 
Rb9 O50 Rb12 80.2(4) 2_645 2_655 ? 
Rb8 O50 Rb12 100.4(5) . 2_655 ? 
Rb10 O50 Rb12 168.4(5) 2_645 2_655 ? 
Si5 O50 Rb7 69.9(6) . 3_666 ? 
Rb9 O50 Rb7 95.9(4) 2_645 3_666 ? 
Rb8 O50 Rb7 171.4(5) . 3_666 ? 
Rb10 O50 Rb7 97.8(4) 2_645 3_666 ? 
Rb12 O50 Rb7 78.6(4) 2_655 3_666 ? 
Si5 O51 Rb6 171.7(9) . 2_645 ? 
Si5 O51 Rb10 89.2(7) . 2_645 ? 
Rb6 O51 Rb10 88.6(4) 2_645 2_645 ? 
Si5 O51 Rb7 86.4(7) . 3_666 ? 
Rb6 O51 Rb7 86.9(4) 2_645 3_666 ? 
Rb10 O51 Rb7 110.8(5) 2_645 3_666 ? 
Si5 O51 Rb11 103.1(7) . . ? 
Rb6 O51 Rb11 84.5(4) 2_645 . ? 
Rb10 O51 Rb11 82.4(4) 2_645 . ? 
Rb7 O51 Rb11 164.0(6) 3_666 . ? 
Si5 O51 Rb11 98.3(7) . 2_655 ? 
Rb6 O51 Rb11 85.1(4) 2_645 2_655 ? 
Rb10 O51 Rb11 168.7(6) 2_645 2_655 ? 
Rb7 O51 Rb11 78.3(3) 3_666 2_655 ? 
Rb11 O51 Rb11 87.6(4) . 2_655 ? 
Si6 O56 Si5 135.1(9) . 2_645 ? 
Si6 O56 Rb12 93.3(7) . . ? 
Si5 O56 Rb12 95.8(6) 2_645 . ? 
Si6 O56 Rb7 145.6(8) . 4_565 ? 
Si5 O56 Rb7 79.3(6) 2_645 4_565 ? 
Rb12 O56 Rb7 82.8(3) . 4_565 ? 
Si6 O56 Rb11 96.6(6) . . ? 
Si5 O56 Rb11 93.8(7) 2_645 . ? 
Rb12 O56 Rb11 154.2(5) . . ? 
Rb7 O56 Rb11 75.6(3) 4_565 . ? 
Si6 O56 Rb10 72.4(5) . . ? 
Si5 O56 Rb10 152.5(7) 2_645 . ? 
Rb12 O56 Rb10 80.8(3) . . ? 
Rb7 O56 Rb10 73.2(3) 4_565 . ? 
Rb11 O56 Rb10 79.7(3) . . ? 
Si6 O60 Rb6 107.6(8) . 2_645 ? 
Si6 O60 Rb11 164.2(9) . 2_655 ? 
Rb6 O60 Rb11 86.8(5) 2_645 2_655 ? 
Si6 O60 Rb10 86.0(7) . . ? 
Rb6 O60 Rb10 162.4(7) 2_645 . ? 
Rb11 O60 Rb10 81.3(4) 2_655 . ? 
Si6 O60 Rb13 87.7(8) . . ? 
Rb6 O60 Rb13 75.1(4) 2_645 . ? 
Rb11 O60 Rb13 89.8(5) 2_655 . ? 
Rb10 O60 Rb13 117.5(6) . . ? 
Si6 O60 Rb11 101.0(8) . . ? 
Rb6 O60 Rb11 80.0(4) 2_645 . ? 
Rb11 O60 Rb11 87.7(5) 2_655 . ? 
Rb10 O60 Rb11 86.6(4) . . ? 
Rb13 O60 Rb11 155.1(6) . . ? 
Si6 O61 Rb8 135.1(8) . 2_655 ? 
Si6 O61 Rb12 104.2(7) . . ? 
Rb8 O61 Rb12 111.2(6) 2_655 . ? 
Si6 O61 Rb5 106.8(8) . 2_645 ? 
Rb8 O61 Rb5 100.7(5) 2_655 2_645 ? 
Rb12 O61 Rb5 88.8(4) . 2_645 ? 
Si6 O61 Rb10 75.7(6) . . ? 
Rb8 O61 Rb10 80.4(4) 2_655 . ? 
Rb12 O61 Rb10 85.6(4) . . ? 
Rb5 O61 Rb10 174.3(6) 2_645 . ? 
Si6 O61 Rb13 76.2(6) . . ? 
Rb8 O61 Rb13 72.1(3) 2_655 . ? 
Rb12 O61 Rb13 172.6(6) . . ? 
Rb5 O61 Rb13 84.0(4) 2_645 . ? 
Rb10 O61 Rb13 101.6(4) . . ? 
 
_diffrn_measured_fraction_theta_max    0.848 
_diffrn_reflns_theta_full              28.22 
_diffrn_measured_fraction_theta_full   0.848 
_refine_diff_density_max    2.298 
_refine_diff_density_min   -1.819 
_refine_diff_density_rms    0.529 
